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MS-NW-7680 chloro(3-cyanopropyl)dimethylsilane C6H12ClNSi (Mass of molecular ion: 161)
Source Temperature: 270 °C Sample Temperature: 170 °C Reservoir, 75 eV
27.0 1.8 28.0 2.4 29.0 1.5 39.0 2.1 41.0 1.9 42.0 1.4 43.0 5.9 53.0 1.0 55.0 1.0 58.0 1.0 59.0 1.4 63.0 12.9 64.0 1.4 65.0 10.7 67.0 2.9 77.0 1.8 78.0 2.6 79.0 4.5 80.0 1.1 81.0 1.5 84.0 1.2 85.0 1.3 90.0 1.7 92.0 2.0 93.0 100.0 94.0 7.8 95.0 35.5 96.0 2.5 97.0 1.4 98.0 13.7 99.0 1.5 104.0 2.0 105.0 1.0 118.0 32.0 119.0 3.6 120.0 12.1 121.0 1.3 126.0 3.2 133.0 37.7 134.0 3.9 135.0 13.3 136.0 1.4 146.0 8.0 148.0 2.9 167.0 1.1 200.0 1.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H12 Cl N Si 0.05 ml : 0.5 ml CDCl3 chloro(3-cyanopropyl)dimethylsilane Assign. Shift(ppm)
A 2.406 B 1.79 C 0.99 D 0.445
Hz ppm Int.
224.13 2.503 43 223.25 2.493 42 216.81 2.421 125 210.38 2.350 81 159.94 1.786 34 152.50 1.703 42 95.81 1.070 80 91.94 1.027 39 87.75 0.980 44 86.25 0.964 40 84.19 0.941 34 79.25 0.885 41 78.63 0.878 38 43.19 0.483 81 39.94 0.446 1000 36.44 0.407 44
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