-
MassMS-NW-4934 chloro(chloromethyl)dimethylsilane C3H8Cl2Si (Mass of molecular ion: 142)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 1.8 29.0 3.3 42.0 1.3 43.0 3.6 63.0 10.3 64.0 1.2 65.0 13.2 66.0 1.0 67.0 3.9 77.0 1.2 78.0 2.0 79.0 13.6 80.0 1.6 81.0 4.6 92.0 1.1 93.0 100.0 94.0 8.0 95.0 35.0 96.0 2.4 97.0 1.2 99.0 12.9 100.0 1.3 101.0 8.7 103.0 1.7 107.0 3.9 109.0 1.3 113.0 1.9 115.0 1.1 127.0 1.9 129.0 1.3 142.0 1.3
parameter in CCl4
90 MHz in CDCl3
-
1H NMR 300 MHz C3 H8 Cl2 Si 10 vol% in CCl4 chloro(chloromethyl)dimethylsilane 
Parameter ppm Hz
D(A) 0.550 D(B) 2.892 SCHMIDBAUR,H. & WALDMANN,S. CHEM.BER. 97, 3381 (1964) J(A,SI-29):7.3HZ. J(B,SI-29):4.6HZ.
Hz ppm Int.867.61 2.892 333 165.00 0.550 1000
-
1H NMR 89.56 MHz C3 H8 Cl2 Si 0.04 ml : 0.5 ml CDCl3 chloro(chloromethyl)dimethylsilane Assign. Shift(ppm)
A 2.948 B 0.548 J(A,SI-29)=4.3HZ J(B,SI-29)=7.2HZ
Hz ppm Int.264.13 2.950 329 52.75 0.589 36 49.13 0.549 1000 45.56 0.509 39
in CDCl3
liquid film
更多供应商
