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网站主页CAS数据库列表 17135-78-3更多图谱2-氯蒽(17135-78-3)核磁图(13CNMR)

2-氯蒽

产品名称 2-氯蒽

CAS号17135-78-3

分子式C14H9Cl

分子量212.67

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  • Mass

    MS-NW-7149          
    2-chloroanthracene
    C14H9Cl             (Mass of molecular ion:    212)
    

       Source Temperature: 150 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          45.0       1.1
          50.0       1.4
          51.0       1.3
          62.0       2.2
          63.0       2.0
          74.0       3.1
          75.0       6.2
          75.5       1.4
          76.0       1.6
          86.0       1.2
          87.0       3.6
          87.5       1.9
          88.0      13.0
          88.5       3.3
          93.0       2.8
          94.0       1.1
          98.0       1.7
          99.0       1.5
         106.0       9.6
         106.5       1.8
         107.0       3.3
         126.0       1.5
         149.0       1.7
         150.0       6.0
         151.0       7.7
         152.0       1.6
         174.0       4.1
         175.0       5.0
         176.0      26.6
         177.0      13.0
         178.0       3.6
         211.0       1.0
         212.0     100.0
         213.0      16.0
         214.0      33.4
         215.0       5.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H9 Cl saturated in CDCl3
    2-chloroanthracene
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 8.387 B *1 8.307 C 7.98 D 7.97 E 7.929 F *2 7.49 G *2 7.47 J 7.373

         Hz     ppm     Int.
    

       3352.05   8.388    634
       3319.82   8.307    641
       3206.18   8.023     30
       3204.47   8.019     43
       3203.49   8.016     40
       3202.03   8.013     48
       3201.17   8.010     48
       3193.60   7.991    552
       3189.94   7.982    333
       3188.72   7.979    387
       3187.38   7.976    373
       3183.96   7.967   1000
       3182.98   7.965    751
       3177.86   7.952     68
       3177.49   7.951     67
       3176.39   7.948     68
       3173.10   7.940    439
       3172.49   7.939    430
       3168.95   7.930     34
       3168.09   7.928     36
       3164.18   7.918    430
       3163.57   7.916    434
       3004.76   7.519     36
       3004.52   7.518     36
       3003.66   7.516     38
       3002.69   7.514     33
       3000.49   7.508     72
       2998.29   7.503    139
       2993.90   7.492    526
       2992.80   7.489    560
       2991.94   7.487    336
       2990.36   7.483    209
       2988.53   7.478    467
       2986.45   7.473    197
       2984.99   7.470    313
       2984.01   7.467    500
       2983.15   7.465    489
       2978.64   7.454    118
       2976.56   7.448     60
       2956.05   7.397     30
       2952.15   7.387    433
       2950.20   7.382    413
       2943.24   7.365    385
       2941.16   7.360    384
    

in CDCl3



KBr disc



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