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MassMS-NW-7553 2-chloro-9,10-diphenylanthracene C26H17Cl (Mass of molecular ion: 364)
Source Temperature: 210 °C Sample Temperature: 150 °C Direct, 75 eV
136.0 1.0 137.0 2.1 138.0 1.1 143.5 1.8 149.0 3.0 149.5 1.3 150.0 4.7 150.5 1.5 151.0 2.1 155.5 1.8 156.0 1.3 156.5 7.4 157.0 3.8 157.5 1.0 161.0 1.9 161.5 1.2 162.0 5.9 162.5 2.6 163.0 9.9 163.5 5.0 164.0 4.7 164.5 3.7 182.0 1.6 224.0 1.1 248.0 1.4 249.0 1.0 250.0 5.6 251.0 2.3 252.0 11.7 253.0 2.8 274.0 1.5 286.0 5.6 287.0 4.5 288.0 2.6 289.0 2.0 298.0 1.8 299.0 1.0 300.0 2.7 301.0 1.4 302.0 1.7 313.0 3.6 314.0 1.7 322.0 1.4 323.0 1.1 324.0 5.9 325.0 2.9 326.0 17.8 327.0 16.9 328.0 17.5 329.0 10.1 330.0 3.4 362.0 1.1 363.0 3.5 364.0 100.0 365.0 29.7 366.0 36.0 367.0 9.2 368.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C26 H17 Cl 0.038 g : 0.5 ml CDCl3 2-chloro-9,10-diphenylanthracene 
Assign. Shift(ppm)
A 7.67 to 7.66 B 7.61 C 7.58 D 7.55 E 7.438 F 7.324 G 7.217
Hz ppm Int.3071.29 7.685 252 3070.56 7.684 294 3068.73 7.679 259 3067.75 7.677 304 3066.89 7.674 297 3066.16 7.673 311 3064.58 7.669 381 3063.35 7.666 399 3061.04 7.660 720 3059.33 7.656 683 3057.62 7.651 430 3056.88 7.649 367 3054.81 7.644 482 3048.95 7.630 160 3047.73 7.626 162 3045.41 7.621 524 3044.92 7.619 492 3042.48 7.613 272 3040.77 7.609 240 3039.31 7.605 256 3037.11 7.600 369 3035.64 7.596 611 3034.06 7.592 415 3032.84 7.589 299 3030.52 7.583 640 3028.56 7.579 732 3026.12 7.572 255 3023.44 7.566 661 3022.71 7.564 677 3021.00 7.560 371 3020.14 7.557 285 3018.31 7.553 439 3016.72 7.549 321 3015.63 7.546 349 3011.47 7.536 297 3008.06 7.527 154 2977.91 7.452 620 2976.44 7.448 1000 2974.85 7.444 682 2972.53 7.438 291 2971.44 7.436 372 2969.97 7.432 695 2968.51 7.428 755 2967.04 7.425 374 2931.27 7.335 428 2930.79 7.334 407 2928.83 7.329 287 2926.88 7.324 318 2925.17 7.320 304 2923.22 7.315 271 2921.14 7.310 400 2889.89 7.232 360 2887.70 7.226 343 2880.49 7.208 343 2878.42 7.203 321
in CDCl3
KBr disc
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