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MassMS-NW-5441 tridodecyl trithiophosphite C36H75PS3 (Mass of molecular ion: 634)
Source Temperature: 190 °C Sample Temperature: 140 °C Direct, 75 eV
27.0 17.4 28.0 3.9 29.0 35.2 39.0 14.1 40.0 2.5 41.0 72.6 42.0 13.8 43.0 100.0 44.0 3.6 45.0 3.9 46.0 1.2 47.0 8.4 53.0 5.7 54.0 7.0 55.0 61.7 56.0 21.8 57.0 92.4 58.0 4.2 59.0 2.0 60.0 5.6 61.0 5.9 63.0 4.4 65.0 1.1 67.0 10.5 68.0 8.1 69.0 37.4 70.0 16.3 71.0 44.5 72.0 2.7 73.0 2.4 74.0 1.0 79.0 1.5 81.0 5.8 82.0 7.9 83.0 22.5 84.0 10.0 85.0 25.3 86.0 1.9 87.0 12.7 88.0 2.2 89.0 4.9 95.0 3.3 96.0 4.4 97.0 15.0 98.0 6.5 99.0 6.8 101.0 6.8 103.0 1.1 105.0 1.3 109.0 1.5 110.0 1.7 111.0 6.9 112.0 3.6 113.0 4.4 115.0 2.8 119.0 1.0 125.0 2.9 126.0 1.8 127.0 2.2 129.0 2.1 139.0 1.3 140.0 2.9 143.0 1.6 145.0 1.6 157.0 1.2 159.0 1.1 168.0 5.5 169.0 1.6 173.0 1.7 187.0 1.2 199.0 4.7 200.0 7.3 201.0 62.3 202.0 14.6 203.0 4.7 229.0 3.3 230.0 1.0 231.0 5.5 232.0 1.7 233.0 1.3 234.0 1.4 263.0 1.0 264.0 3.6 265.0 8.1 266.0 1.9 267.0 1.4 297.0 1.5 298.0 1.7 299.0 1.2 402.0 3.6 403.0 1.2 432.0 1.5 433.0 16.7 434.0 5.5 435.0 2.4 465.0 1.0 466.0 2.1 467.0 1.3 634.0 3.9 635.0 1.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C36 H75 P S3 0.04 ml : 0.5 ml CDCl3 tridodecyl trithiophosphite 
Assign. Shift(ppm)
A 2.81 B 1.70 C 1.26 D 0.89
Hz ppm Int.126.44 1.412 34 124.19 1.387 45 121.56 1.358 57 112.88 1.261 1000 84.13 0.940 45 81.88 0.915 36 81.25 0.908 35 78.94 0.882 146 72.94 0.815 32
in CDCl3
CCl4 solution
liquid film
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