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MassMS-NW-1773 triphenyl phosphate C18H15O4P (Mass of molecular ion: 326)
Source Temperature: 210 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 1.9 27.0 1.4 28.0 1.6 38.0 1.8 39.0 17.3 40.0 1.0 47.0 4.8 50.0 4.3 51.0 21.0 52.0 1.3 63.0 4.3 64.0 3.1 65.0 36.1 66.0 4.0 74.0 1.1 75.0 1.6 76.0 2.5 77.0 63.4 78.0 4.8 81.0 1.2 92.0 1.8 93.0 7.7 94.0 23.8 95.0 2.3 100.0 1.3 109.0 1.3 115.0 3.5 139.0 4.9 140.0 6.6 141.0 8.4 142.0 3.5 151.0 2.1 152.0 6.7 153.0 2.4 156.0 2.7 157.0 1.0 168.0 10.9 169.0 20.0 170.0 34.0 171.0 4.5 187.0 1.5 215.0 21.6 216.0 3.1 217.0 1.4 226.0 1.2 227.0 3.2 228.0 15.5 229.0 6.6 230.0 1.1 231.0 2.1 232.0 15.1 233.0 30.0 234.0 4.0 244.0 1.1 245.0 2.1 246.0 4.7 249.0 5.3 325.0 63.2 326.0 100.0 327.0 18.7 328.0 2.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C18 H15 O4 P 0.053 g : 0.5 ml CDCl3 triphenyl phosphate 
Assign. Shift(ppm)
A 7.05 to 7.46
Hz ppm Int.667.00 7.448 31 666.50 7.442 41 665.63 7.433 51 665.06 7.426 45 664.13 7.416 37 663.50 7.409 39 662.88 7.402 33 660.94 7.380 55 659.31 7.362 95 657.69 7.344 117 657.00 7.336 187 656.13 7.327 184 655.56 7.320 166 654.94 7.313 167 653.56 7.298 88 651.38 7.274 1000 650.25 7.261 972 649.81 7.256 952 646.19 7.216 193 644.88 7.201 212 643.88 7.190 120 642.63 7.176 135 642.06 7.170 124 641.31 7.161 130 640.88 7.156 129 636.06 7.103 42 635.06 7.091 36 634.88 7.089 36
in CDCl3
CCl4 solution
KBr disc
nujol mull
4880 A,200 M,powder
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