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MassMS-NW-8329 2-methoxypyridine C6H7NO (Mass of molecular ion: 109)
Source Temperature: 260 °C Sample Temperature: 130 °C Reservoir, 75 eV
15.0 3.6 26.0 3.2 27.0 5.7 28.0 5.9 29.0 1.7 37.0 4.3 38.0 12.3 39.0 31.3 40.0 4.4 41.0 1.7 42.0 4.2 49.0 1.6 50.0 8.4 51.0 20.7 52.0 55.5 53.0 11.4 54.0 1.4 55.0 1.8 64.0 2.9 65.0 2.8 66.0 7.1 67.0 1.1 75.0 1.2 76.0 1.8 78.0 22.6 79.0 100.0 80.0 31.5 81.0 2.8 93.0 1.4 106.0 1.7 108.0 73.5 109.0 60.2 110.0 4.5 113.0 3.5 115.0 1.1
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C6 H7 N O 0.05 ml : 0.5 ml CDCl3 2-methoxypyridine 
Assign. Shift(ppm)
A 8.152 B 7.505 C 6.810 E 6.715 E 3.917
Hz ppm Int.733.88 8.195 50 733.19 8.187 52 732.00 8.174 56 728.88 8.139 55 728.31 8.133 56 726.94 8.117 57 681.38 7.609 43 679.38 7.586 40 674.25 7.529 59 673.06 7.516 64 672.25 7.507 58 671.06 7.493 50 666.00 7.437 63 664.00 7.415 56 616.50 6.884 62 615.56 6.874 67 611.44 6.828 60 610.50 6.817 77 609.44 6.805 63 608.50 6.795 60 606.19 6.769 98 605.31 6.759 133 604.38 6.749 99 603.50 6.739 55 597.88 6.676 69 597.06 6.667 94 350.88 3.918 1000
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1H NMR 399.65 MHz C6 H7 N O 0.05 ml : 0.5 ml CDCl3 2-methoxypyridine Assign. Shift(ppm)
A 8.157 B 7.517 C 6.824 D 6.724 E 3.921
Hz ppm Int.3263.92 8.167 94 3263.18 8.166 102 3261.96 8.163 105 3261.23 8.161 99 3258.91 8.155 96 3258.06 8.153 103 3256.84 8.150 102 3256.10 8.148 97 3013.06 7.540 114 3011.11 7.535 121 3006.10 7.522 128 3004.76 7.519 145 3004.03 7.517 145 3002.69 7.514 130 2997.68 7.501 132 2995.61 7.496 125 2733.64 6.841 127 2732.79 6.838 133 2728.64 6.828 131 2727.66 6.826 144 2726.56 6.823 133 2725.71 6.821 129 2721.56 6.810 121 2720.58 6.808 127 2692.14 6.737 156 2691.28 6.735 238 2690.31 6.732 152 2683.84 6.716 137 2682.86 6.714 222 2682.01 6.711 144 1567.02 3.921 1000
in CDCl3
liquid film
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