2,6-二甲氧基吡啶

产品名称 2,6-二甲氧基吡啶

CAS号6231-18-1

分子式C7H9NO2

分子量139.15

¹³CNMR

Mass

MS-NW-9443          
2,6-dimethoxypyridine
C7H9NO2             (Mass of molecular ion:    139)

   Source Temperature: 240 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       4.4
      26.0       2.1
      27.0       2.5
      28.0       2.4
      29.0       1.2
      37.0       2.6
      38.0      10.7
      39.0      25.3
      40.0       2.1
      41.0       3.1
      42.0       3.1
      50.0       1.8
      51.0       1.9
      52.0       4.3
      53.0       5.4
      54.0       3.8
      55.0       5.9
      64.0       5.8
      65.0      10.2
      66.0      16.3
      67.0       2.5
      68.0       3.6
      69.5       1.0
      70.0       2.2
      77.0       1.4
      78.0       7.3
      79.0       4.5
      80.0      14.5
      81.0       5.2
      82.0       1.4
      91.0       5.3
      92.0       1.6
      93.0      13.1
      94.0      21.8
      95.0       4.5
      96.0       7.5
     106.0       3.2
     107.0       1.1
     108.0      14.2
     109.0      38.3
     110.0      28.4
     111.0       2.0
     120.0       2.7
     121.0       6.1
     122.0       1.2
     123.0       1.4
     124.0      10.3
     138.0     100.0
     139.0      98.3
     140.0       8.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₉ N O₂	0.05 ml : 0.5 ml CDCl₃
2,6-dimethoxypyridine

    Assign.     Shift(ppm)

      A             7.445
      B             6.277
      C             3.891

     Hz     ppm     Int.

   2983.64   7.466    185
   2975.83   7.447    312
   2967.90   7.427    195
   2512.57   6.287    532
   2504.76   6.268    516
   1626.83   4.071     28
   1555.30   3.892   1000
   1481.45   3.707     27

in CDCl3

liquid film

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