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MassMS-NW-7747 alpha,alpha-diphenyl-4-pyridinemethanol C18H15NO (Mass of molecular ion: 261)
Source Temperature: 180 °C Sample Temperature: 130 °C Direct, 75 eV
27.0 2.1 28.0 1.9 39.0 3.7 45.0 1.0 50.0 5.6 51.0 27.1 52.0 5.0 53.0 1.6 62.0 1.4 63.0 3.6 65.0 1.1 74.0 2.0 75.0 2.6 76.0 3.7 77.0 63.1 78.0 35.8 79.0 36.4 80.0 4.9 87.0 1.7 88.0 1.2 89.0 1.7 91.0 1.9 94.5 1.5 101.0 1.6 102.0 1.5 104.0 1.0 105.0 100.0 106.0 44.9 106.5 1.1 107.0 5.2 113.0 1.1 115.0 2.3 121.5 1.0 126.0 1.6 127.0 3.4 128.0 2.7 139.0 3.6 140.0 1.5 151.0 1.1 152.0 3.3 153.0 1.8 154.0 3.8 155.0 8.8 156.0 15.2 157.0 2.1 163.0 1.3 164.0 1.1 165.0 5.7 166.0 3.3 167.0 4.9 168.0 1.4 181.0 1.8 182.0 4.1 183.0 94.1 184.0 36.0 185.0 4.8 189.0 1.7 202.0 1.4 213.0 1.7 214.0 1.0 215.0 2.4 216.0 1.0 240.0 1.0 241.0 2.2 242.0 2.8 243.0 4.9 244.0 3.7 245.0 4.2 246.0 1.0 258.0 1.0 259.0 1.8 260.0 5.3 261.0 58.9 262.0 12.6 263.0 1.7
400 MHz in DMSO-d6 at 60C
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1H NMR 399.65 MHz C18 H15 N O 0.026 g : 0.5 ml DMSO-d6 at 60 C alpha,alpha-diphenyl-4-pyridinemethanol 
Assign. Shift(ppm)
A 8.504 B 7.31 C 7.27 D 7.24 E 7.21 F 6.57
Hz ppm Int.3400.63 8.510 182 3395.75 8.497 182 2943.85 7.367 33 2943.48 7.366 34 2942.63 7.364 36 2939.09 7.355 73 2933.47 7.341 181 2931.88 7.337 274 2930.18 7.332 184 2925.05 7.320 646 2923.34 7.315 420 2918.95 7.304 324 2917.60 7.301 650 2911.13 7.285 217 2909.55 7.281 371 2908.08 7.277 303 2905.03 7.269 169 2902.47 7.263 397 2899.41 7.255 147 2894.41 7.243 404 2890.75 7.234 781 2889.16 7.230 1000 2884.03 7.217 321 2882.32 7.213 523 2881.10 7.210 419 2875.37 7.195 32 2626.83 6.573 295
DMSO-d6
KBr disc
nujol mull
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