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MassMS-NW-8641 dichlorodiphenylgermane C12H10Cl2Ge (Mass of molecular ion: 298)
Source Temperature: 260 °C Sample Temperature: 130 °C Reservoir, 75 eV
18.0 2.0 27.0 3.5 36.0 2.0 38.0 1.0 39.0 3.2 50.0 14.5 51.0 64.4 52.0 4.1 63.0 1.1 74.0 3.8 75.0 4.2 76.0 7.8 77.0 100.0 78.0 8.0 95.0 2.3 97.0 3.1 98.0 1.1 99.0 4.2 101.0 1.0 105.0 18.0 107.0 29.9 108.0 6.9 109.0 39.6 110.0 2.4 111.0 17.1 112.0 1.1 113.0 2.2 121.0 2.0 123.0 2.7 125.0 2.3 126.0 1.1 127.0 1.3 147.0 7.2 149.0 9.6 150.0 3.7 151.0 13.7 152.0 10.7 153.0 8.4 154.0 79.6 155.0 10.4 182.0 8.6 184.0 14.1 185.0 4.5 186.0 19.2 187.0 2.5 188.0 8.2 190.0 1.1 217.0 8.7 219.0 17.2 220.0 4.7 221.0 24.2 222.0 5.0 223.0 15.1 224.0 3.2 225.0 5.2 226.0 3.1 227.0 1.7 259.0 32.5 260.0 5.3 261.0 54.1 262.0 20.4 263.0 73.0 264.0 13.9 265.0 31.9 266.0 4.3 267.0 4.6 294.0 14.3 295.0 1.9 296.0 28.5 297.0 9.2 298.0 39.8 299.0 8.8 300.0 24.3 301.0 3.7 302.0 6.3 303.0 1.3 305.0 1.4 307.0 1.7 309.0 1.2 340.0 1.4 342.0 2.0 344.0 1.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C12 H10 Cl2 Ge ca 10 mg : 0.5 ml CDCl3 dichlorodiphenylgermane 
Assign. Shift(ppm)
A 7.67 B 7.45 C 7.42 CONFIRMED BY LAOCN PROGRAM
Hz ppm Int.698.94 7.805 37 697.44 7.788 50 694.44 7.754 271 692.00 7.727 358 688.56 7.689 544 687.25 7.674 277 686.06 7.661 365 684.81 7.647 528 682.44 7.620 195 680.38 7.597 115 679.69 7.590 114 678.69 7.579 123 675.88 7.547 70 672.25 7.507 161 670.94 7.492 242 668.38 7.463 1000 666.06 7.438 836 663.44 7.408 433 663.00 7.403 428 661.56 7.387 491 658.88 7.357 210 658.06 7.348 187 655.56 7.320 85 654.94 7.313 81 653.63 7.299 82 652.13 7.282 44
in CDCl3
liquid film
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