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网站主页CAS数据库列表 1581-13-1更多图谱2-氨基-2'-氟苯甲酮(1581-13-1)核磁图(1HNMR)

2-氨基-2'-氟苯甲酮

产品名称 2-氨基-2'-氟苯甲酮

CAS号1581-13-1

分子式C13H10FNO

分子量215.22


  • Mass

    MS-IW-0787          
    2-amino-2'-fluorobenzophenone
    C13H10FNO           (Mass of molecular ion:    215)
    

       Source Temperature: 140 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          28.0       1.0
          39.0       3.7
          51.0       1.0
          52.0       1.2
          63.0       1.9
          64.0       1.8
          65.0      15.2
          66.0       1.7
          75.0       4.4
          83.5       3.5
          85.0       1.0
          91.0       1.3
          92.0      22.2
          92.5       1.7
          93.0       2.1
          95.0      12.6
          96.0       1.0
         107.0       1.1
         107.5       3.8
         119.0       2.2
         120.0      39.7
         121.0       3.3
         123.0      15.2
         124.0       1.2
         139.0       1.6
         166.0       3.1
         167.0       3.9
         168.0       1.1
         185.0       3.0
         186.0       6.6
         187.0       1.2
         194.0       2.9
         195.0      10.2
         196.0      17.7
         197.0       2.8
         198.0      11.2
         199.0       1.6
         214.0      69.6
         215.0     100.0
         216.0      14.2
         217.0       1.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H10 F N O 0.038 g : 0.5 ml CDCl3
    2-amino-2'-fluorobenzophenone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.455 B 7.409 C 7.314 D 7.325 E 7.228 F 7.142 G 6.703 J 6.568 K 6.39

         Hz     ppm     Int.
    

       2989.75   7.481    199
       2987.92   7.477    233
       2984.50   7.468    217
       2982.67   7.464    414
       2981.45   7.461    299
       2980.59   7.459    340
       2979.61   7.456    310
       2977.17   7.450    290
       2976.20   7.448    297
       2975.34   7.445    359
       2974.37   7.443    461
       2972.29   7.438    337
       2968.38   7.428    468
       2966.92   7.424    497
       2960.82   7.409    601
       2959.72   7.406    485
       2959.35   7.405    481
       2953.98   7.392    483
       2952.15   7.387    388
       2931.15   7.335    305
       2929.32   7.330    454
       2927.37   7.325    372
       2922.97   7.314    335
       2921.26   7.310    507
       2919.56   7.306    762
       2918.09   7.302    436
       2915.53   7.296     59
       2912.60   7.288    532
       2911.25   7.285    728
       2909.79   7.281    431
       2906.98   7.274     52
       2904.30   7.268    488
       2902.71   7.264    410
       2900.02   7.257     46
       2896.12   7.247    626
       2895.02   7.244    664
       2892.58   7.238     49
       2891.60   7.236     53
       2888.67   7.229    962
       2887.57   7.226    978
       2884.64   7.218     51
       2884.03   7.217     45
       2881.10   7.210    455
       2880.00   7.207    460
       2863.40   7.165    452
       2862.30   7.163    436
       2854.74   7.144    456
       2853.76   7.141    757
       2852.66   7.138    477
       2845.34   7.120    400
       2844.36   7.118    390
       2683.72   6.716    760
       2683.23   6.714    794
       2682.62   6.713    820
       2679.81   6.706     45
       2675.29   6.695    726
       2674.93   6.694    751
       2674.19   6.692    756
       2632.81   6.588    566
       2631.71   6.586    538
       2629.52   6.580     40
       2629.03   6.579     40
       2625.73   6.571    606
       2624.76   6.568   1000
       2623.66   6.565    542
       2621.46   6.560     49
       2621.09   6.559     48
       2620.36   6.557     43
       2619.75   6.556     42
       2617.68   6.550    532
       2616.58   6.548    486
       2552.25   6.387    357
    

in CDCl3



KBr disc



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