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MS-IW-0787 2-amino-2'-fluorobenzophenone C13H10FNO (Mass of molecular ion: 215)
Source Temperature: 140 °C Sample Temperature: 100 °C Direct, 75 eV
28.0 1.0 39.0 3.7 51.0 1.0 52.0 1.2 63.0 1.9 64.0 1.8 65.0 15.2 66.0 1.7 75.0 4.4 83.5 3.5 85.0 1.0 91.0 1.3 92.0 22.2 92.5 1.7 93.0 2.1 95.0 12.6 96.0 1.0 107.0 1.1 107.5 3.8 119.0 2.2 120.0 39.7 121.0 3.3 123.0 15.2 124.0 1.2 139.0 1.6 166.0 3.1 167.0 3.9 168.0 1.1 185.0 3.0 186.0 6.6 187.0 1.2 194.0 2.9 195.0 10.2 196.0 17.7 197.0 2.8 198.0 11.2 199.0 1.6 214.0 69.6 215.0 100.0 216.0 14.2 217.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H10 F N O 0.038 g : 0.5 ml CDCl3 2-amino-2'-fluorobenzophenone Assign. Shift(ppm)
A 7.455 B 7.409 C 7.314 D 7.325 E 7.228 F 7.142 G 6.703 J 6.568 K 6.39
Hz ppm Int.
2989.75 7.481 199 2987.92 7.477 233 2984.50 7.468 217 2982.67 7.464 414 2981.45 7.461 299 2980.59 7.459 340 2979.61 7.456 310 2977.17 7.450 290 2976.20 7.448 297 2975.34 7.445 359 2974.37 7.443 461 2972.29 7.438 337 2968.38 7.428 468 2966.92 7.424 497 2960.82 7.409 601 2959.72 7.406 485 2959.35 7.405 481 2953.98 7.392 483 2952.15 7.387 388 2931.15 7.335 305 2929.32 7.330 454 2927.37 7.325 372 2922.97 7.314 335 2921.26 7.310 507 2919.56 7.306 762 2918.09 7.302 436 2915.53 7.296 59 2912.60 7.288 532 2911.25 7.285 728 2909.79 7.281 431 2906.98 7.274 52 2904.30 7.268 488 2902.71 7.264 410 2900.02 7.257 46 2896.12 7.247 626 2895.02 7.244 664 2892.58 7.238 49 2891.60 7.236 53 2888.67 7.229 962 2887.57 7.226 978 2884.64 7.218 51 2884.03 7.217 45 2881.10 7.210 455 2880.00 7.207 460 2863.40 7.165 452 2862.30 7.163 436 2854.74 7.144 456 2853.76 7.141 757 2852.66 7.138 477 2845.34 7.120 400 2844.36 7.118 390 2683.72 6.716 760 2683.23 6.714 794 2682.62 6.713 820 2679.81 6.706 45 2675.29 6.695 726 2674.93 6.694 751 2674.19 6.692 756 2632.81 6.588 566 2631.71 6.586 538 2629.52 6.580 40 2629.03 6.579 40 2625.73 6.571 606 2624.76 6.568 1000 2623.66 6.565 542 2621.46 6.560 49 2621.09 6.559 48 2620.36 6.557 43 2619.75 6.556 42 2617.68 6.550 532 2616.58 6.548 486 2552.25 6.387 357
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