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网站主页CAS数据库列表 342-24-5更多图谱邻氟二苯甲酮(342-24-5)核磁图(13CNMR)

邻氟二苯甲酮

产品名称 邻氟二苯甲酮

CAS号342-24-5

分子式C13H9FO

分子量200.21

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  • Mass

    MS-NW-8627          
    2-fluorobenzophenone
    C13H9FO             (Mass of molecular ion:    200)
    

       Source Temperature: 260 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          39.0       1.1
          50.0       5.5
          51.0      16.1
          63.0       1.0
          69.0       1.9
          74.0       2.8
          75.0      12.3
          76.0       4.2
          77.0      48.3
          78.0       3.4
          85.0       1.3
          86.0       2.3
          94.0       2.0
          95.0      25.2
          96.0       1.9
         105.0     100.0
         106.0       7.8
         123.0      63.1
         124.0       5.0
         133.0       1.0
         151.0       1.6
         152.0       1.0
         170.0       2.5
         171.0       1.6
         172.0       2.2
         180.0       4.4
         199.0       3.4
         200.0      58.8
         201.0       8.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H9 F O 0.05 ml : 0.5 ml CDCl3
    2-fluorobenzophenone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.828 B 7.56 C 7.53 D 7.49 E 7.44 G 7.235 J 7.128 C,D,G AND J WERE CONFIRMED BY LAOCN PROGRAM.

         Hz     ppm     Int.
    

       3135.74   7.847    125
       3134.03   7.842    446
       3132.81   7.839    809
       3131.47   7.836    694
       3127.69   7.827    199
       3125.61   7.821    637
       3124.39   7.818    938
       3123.05   7.815    615
       3034.30   7.593     32
       3031.86   7.587    159
       3030.52   7.583    291
       3029.17   7.580    183
       3026.86   7.574     63
       3025.02   7.570    214
       3023.07   7.565    583
       3021.24   7.560    261
       3019.53   7.556     80
       3016.97   7.550    410
       3015.75   7.546    556
       3014.53   7.543    489
       3011.84   7.537     71
       3009.28   7.530    361
       3007.45   7.526    460
       3005.00   7.520    229
       3003.17   7.515    203
       3001.95   7.512    284
       3000.00   7.507    423
       2997.56   7.501    298
       2996.70   7.499    261
       2995.73   7.496    224
       2994.87   7.494    226
       2992.31   7.488    275
       2991.46   7.486    263
       2990.48   7.483    237
       2989.26   7.480    316
       2987.43   7.476    217
       2984.01   7.467    284
       2982.79   7.464    247
       2981.08   7.460    765
       2979.61   7.456    400
       2973.14   7.440   1000
       2971.92   7.437    429
       2967.53   7.426    234
       2965.82   7.422    505
       2965.21   7.420    409
       2964.36   7.418    194
       2959.35   7.405     30
       2902.34   7.263     34
       2898.44   7.253    483
       2897.34   7.250    487
       2894.41   7.243     45
       2893.31   7.240     53
       2890.87   7.234    685
       2889.89   7.232    744
       2885.86   7.221     39
       2883.30   7.215    330
       2882.32   7.213    366
       2858.03   7.152    297
       2857.30   7.150    311
       2849.73   7.131    288
       2848.51   7.128    454
       2847.41   7.125    343
       2839.72   7.106    263
       2839.11   7.104    270
    

in CDCl3



liquid film