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MS-NW-2386 2-(p-tolyloxy)ethanol C9H12O2 (Mass of molecular ion: 152)
Source Temperature: 280 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.4 27.0 5.2 28.0 1.2 29.0 4.3 31.0 1.3 39.0 5.3 41.0 1.1 43.0 2.8 44.0 2.4 45.0 8.3 50.0 2.4 51.0 5.0 52.0 2.6 53.0 2.8 63.0 2.9 65.0 7.7 77.0 10.3 78.0 2.7 79.0 8.7 80.0 5.9 89.0 2.4 90.0 6.5 91.0 19.7 92.0 1.8 93.0 2.2 107.0 53.2 108.0 100.0 109.0 10.3 121.0 4.7 152.0 35.3 153.0 3.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H12 O2 0.048 g : 0.5 ml CDCl3 2-(p-tolyloxy)ethanol Assign. Shift(ppm)
A 7.05 B 6.81 C 4.01 D 3.92 E 2.43 F 2.28
Hz ppm Int.
638.00 7.124 141 637.38 7.117 164 635.81 7.100 71 635.13 7.092 61 631.50 7.052 68 630.94 7.045 79 629.13 7.025 320 628.56 7.019 290 626.63 6.997 61 626.06 6.991 56 615.19 6.870 58 612.69 6.842 447 610.31 6.815 120 606.13 6.768 76 603.94 6.744 216 366.50 4.093 50 364.38 4.069 80 363.44 4.059 75 361.25 4.034 126 360.19 4.022 130 359.44 4.014 184 357.19 3.989 378 356.63 3.983 360 353.69 3.950 371 353.13 3.943 385 350.94 3.919 182 350.13 3.910 148 349.13 3.899 129 346.88 3.874 81 346.00 3.864 81 343.88 3.840 54 217.50 2.429 462 203.75 2.276 1000
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