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网站主页CAS数据库列表 3101-60-8更多图谱对叔丁基苯基1-(2,3-环氧)丙基醚(3101-60-8)核磁图(13CNMR)

对叔丁基苯基1-(2,3-环氧)丙基醚

产品名称 对叔丁基苯基1-(2,3-环氧)丙基醚

CAS号3101-60-8

分子式C13H18O2

分子量206.28

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  • Mass

    MS2017-05423CM      
    p-tert-butylphenyl 2,3-epoxypropyl ether
    C13H18O2            (Mass of molecular ion:    206)
    

       Source Temperature: 250 °C
       Sample Temperature:  20 °C
       Direct, 70 eV
    

          27.0       2.0
          29.0       3.1
          31.0       2.8
          39.0       1.6
          41.0       4.0
          57.0       7.8
          65.0       1.5
          77.0       3.2
          78.0       1.0
          79.0       1.4
          91.0       5.4
          95.0       2.9
         105.0       2.0
         107.0       8.9
         115.0       1.3
         117.0       1.2
         119.0       1.7
         133.0       1.6
         134.0       1.1
         135.0      32.4
         136.0       3.2
         147.0       1.0
         161.0       1.6
         191.0     100.0
         192.0      13.0
         193.0       1.2
         206.0      23.7
         207.0       3.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H18 O2 0.05 ml : 0.5 ml CDCl3
    p-tert-butylphenyl 2,3-epoxypropyl ether
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.287 B 6.848 C *1 4.159 D *1 3.914 E 3.303 F 2.844 G 2.703 J 1.286 J(C,D)=-11.0HZ J(C,E)=3.2HZ J(D,E)=5.7HZ J(E,G)=2.7HZ J(E,F)=4.3HZ J(F,G)=5.0HZ

         Hz     ppm     Int.
    

       2917.36   7.300    178
       2915.04   7.294     68
       2910.64   7.283     66
       2908.33   7.278    206
       2905.15   7.270     32
       2741.33   6.860    190
       2739.01   6.854     69
       2734.62   6.843     60
       2732.30   6.837    181
       2729.13   6.829     32
       1670.17   4.180     60
       1666.99   4.172     63
       1659.18   4.152     75
       1655.88   4.144     76
       1572.27   3.935     68
       1566.53   3.920     72
       1561.16   3.907     57
       1555.54   3.893     59
       1325.44   3.317     35
       1324.58   3.315     34
       1322.88   3.311     44
       1321.90   3.308     40
       1321.41   3.307     42
       1320.31   3.304     38
       1319.82   3.303     39
       1318.73   3.300     49
       1317.14   3.296     30
       1316.28   3.294     36
       1315.67   3.293     38
       1141.60   2.857     74
       1137.45   2.847     79
       1136.72   2.845    104
       1132.45   2.834     81
       1084.11   2.713     77
       1081.42   2.706     79
       1079.10   2.701     70
       1076.54   2.694     68
        518.68   1.298     81
        514.04   1.287   1000
    

in CDCl3



Liquid film