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MassMS2017-05423CM p-tert-butylphenyl 2,3-epoxypropyl ether C13H18O2 (Mass of molecular ion: 206)
Source Temperature: 250 °C Sample Temperature: 20 °C Direct, 70 eV
27.0 2.0 29.0 3.1 31.0 2.8 39.0 1.6 41.0 4.0 57.0 7.8 65.0 1.5 77.0 3.2 78.0 1.0 79.0 1.4 91.0 5.4 95.0 2.9 105.0 2.0 107.0 8.9 115.0 1.3 117.0 1.2 119.0 1.7 133.0 1.6 134.0 1.1 135.0 32.4 136.0 3.2 147.0 1.0 161.0 1.6 191.0 100.0 192.0 13.0 193.0 1.2 206.0 23.7 207.0 3.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H18 O2 0.05 ml : 0.5 ml CDCl3 p-tert-butylphenyl 2,3-epoxypropyl ether 
Assign. Shift(ppm)
A 7.287 B 6.848 C *1 4.159 D *1 3.914 E 3.303 F 2.844 G 2.703 J 1.286 J(C,D)=-11.0HZ J(C,E)=3.2HZ J(D,E)=5.7HZ J(E,G)=2.7HZ J(E,F)=4.3HZ J(F,G)=5.0HZ
Hz ppm Int.2917.36 7.300 178 2915.04 7.294 68 2910.64 7.283 66 2908.33 7.278 206 2905.15 7.270 32 2741.33 6.860 190 2739.01 6.854 69 2734.62 6.843 60 2732.30 6.837 181 2729.13 6.829 32 1670.17 4.180 60 1666.99 4.172 63 1659.18 4.152 75 1655.88 4.144 76 1572.27 3.935 68 1566.53 3.920 72 1561.16 3.907 57 1555.54 3.893 59 1325.44 3.317 35 1324.58 3.315 34 1322.88 3.311 44 1321.90 3.308 40 1321.41 3.307 42 1320.31 3.304 38 1319.82 3.303 39 1318.73 3.300 49 1317.14 3.296 30 1316.28 3.294 36 1315.67 3.293 38 1141.60 2.857 74 1137.45 2.847 79 1136.72 2.845 104 1132.45 2.834 81 1084.11 2.713 77 1081.42 2.706 79 1079.10 2.701 70 1076.54 2.694 68 518.68 1.298 81 514.04 1.287 1000
in CDCl3
Liquid film
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