图谱信息 供应商 相关产品
网站主页 > CAS数据库列表  > 15121-84-3更多图谱  >2-(2-硝基苯基)乙醇(15121-84-3)核磁图(13CNMR)

2-(2-硝基苯基)乙醇

CAS号15121-84-3

分子式C8H9NO3

分子量167.16

展开


  • Mass

    MS-NW-5585          
    o-nitrophenethyl alcohol
    C8H9NO3             (Mass of molecular ion:    167)
    

       Source Temperature: 270 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          17.0       1.0
          18.0       4.9
          27.0       3.4
          28.0       4.7
          29.0       3.3
          30.0       2.6
          31.0      12.1
          38.0       2.4
          39.0      12.8
          40.0       1.8
          41.0       3.4
          43.0       1.7
          47.0       1.0
          50.0       5.2
          51.0      11.5
          52.0       4.1
          53.0       3.0
          59.0       1.4
          61.0       1.0
          62.0       3.2
          63.0      10.2
          64.0       6.1
          65.0      35.1
          66.0       5.5
          67.0       1.1
          74.0       1.6
          75.0       2.1
          76.0       2.7
          77.0      28.8
          78.0      12.1
          79.0       4.1
          80.0       1.0
          89.0      16.4
          90.0      12.3
          91.0      18.8
          92.0      44.7
          93.0       7.5
          94.0       1.1
         101.0       1.0
         102.0       1.9
         103.0       4.3
         104.0       3.0
         105.0       2.7
         106.0       2.1
         107.0       1.2
         116.0       1.1
         117.0      10.7
         118.0       1.9
         119.0       1.4
         120.0     100.0
         121.0       9.4
         132.0       3.8
         133.0       1.6
         134.0       1.1
         137.0      40.9
         138.0       3.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H9 N O3 0.05 ml : 0.5 ml CDCl3
    o-nitrophenethyl alcohol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.878 B 7.530 C 7.411 D 7.359 E 3.860 F 3.113 G 3.07

         Hz     ppm     Int.
    

       3153.32   7.891    255
       3152.10   7.888    278
       3145.14   7.870    281
       3143.92   7.867    305
       3018.55   7.553    123
       3017.21   7.550    128
       3011.11   7.535    261
       3009.77   7.532    282
       3003.54   7.516    211
       3002.20   7.513    211
       2965.94   7.422    251
       2964.84   7.419    308
       2958.13   7.402    201
       2957.03   7.400    222
       2949.34   7.380    192
       2947.88   7.377    168
       2941.16   7.360    249
       2933.84   7.342    148
       2932.37   7.338    138
       1549.56   3.878    496
       1542.85   3.861   1000
       1536.38   3.845    557
       1251.22   3.131    389
       1244.51   3.115    730
       1237.92   3.098    384
       1225.22   3.066    257
    

in CDCl3



liquid film