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MS-IW-1255 2-nitroethanol C2H5NO3 (Mass of molecular ion: 91)
Source Temperature: 230 °C Sample Temperature: 160 °C Reservoir, 75 eV
14.0 1.5 15.0 7.7 17.0 1.8 18.0 9.3 19.0 13.8 26.0 2.6 27.0 45.5 28.0 14.9 29.0 20.7 30.0 21.3 31.0 26.0 32.0 1.1 39.0 1.0 41.0 4.3 42.0 4.1 43.0 28.2 44.0 24.4 45.0 100.0 46.0 7.3 57.0 1.4 58.0 1.1 59.0 4.4 61.0 10.0 62.0 1.7 73.0 2.4 74.0 1.5 75.0 1.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C2 H5 N O3 0.05 ml : 0.5 ml CDCl3 2-nitroethanol Assign. Shift(ppm)
A 4.545 B 4.110 C 3.59
Hz ppm Int.
1821.29 4.558 965 1818.85 4.552 393 1817.87 4.549 575 1816.41 4.546 848 1814.70 4.541 548 1813.72 4.539 410 1811.52 4.533 1000 1647.46 4.123 847 1644.17 4.115 455 1642.46 4.110 783 1640.99 4.107 459 1637.70 4.098 733 1628.30 4.075 29 1435.06 3.591 207
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