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网站主页CAS数据库列表 14937-45-2更多图谱十六烷基三丁基溴化磷(14937-45-2)Raman光谱

十六烷基三丁基溴化磷

产品名称 十六烷基三丁基溴化磷

CAS号14937-45-2

分子式C28H60BrP

分子量507.67

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  • Mass

    MS-NW-7198          
    tributylhexadecylphosphonium bromide
    C28H60BrP           (Mass of molecular ion:    506)
    

       Source Temperature: 200 °C
       Sample Temperature: 230 °C
       Direct, 75 eV
    

          18.0       1.7
          27.0       2.3
          28.0       1.7
          29.0       5.4
          39.0       1.8
          41.0       9.7
          42.0       1.8
          43.0      10.1
          48.0       1.1
          55.0       8.0
          56.0       2.8
          57.0       5.9
          59.0       1.1
          61.0       4.7
          62.0      11.3
          67.0       1.1
          69.0       3.1
          70.0       1.5
          71.0       1.7
          73.0       1.2
          74.0       1.2
          75.0       1.6
          76.0      17.5
          80.0       2.1
          82.0       2.1
          83.0       1.9
          87.0       1.0
          88.0       1.8
          89.0       2.6
          90.0       4.1
          97.0       1.4
         102.0       1.9
         103.0       2.0
         104.0      10.2
         105.0       1.4
         116.0       1.6
         117.0       1.9
         118.0       9.7
         131.0       3.5
         132.0       2.5
         145.0       2.0
         146.0      11.3
         147.0       2.4
         159.0       1.4
         160.0       6.1
         173.0       6.2
         174.0       2.3
         187.0       1.9
         188.0       1.0
         201.0       4.0
         202.0       5.1
         203.0       1.0
         215.0       3.0
         216.0       1.0
         229.0       5.7
         230.0       1.3
         243.0       2.2
         257.0       2.7
         271.0       2.6
         272.0       1.1
         285.0       2.7
         286.0       1.0
         299.0       2.9
         313.0       3.4
         314.0       2.8
         327.0       2.8
         328.0       1.4
         341.0       4.4
         342.0       1.3
         355.0       1.7
         369.0       4.5
         370.0       4.0
         371.0       1.4
         383.0       1.1
         397.0       3.4
         398.0       1.1
         425.0       6.6
         426.0       2.9
         427.0     100.0
         428.0      30.7
         429.0       4.9
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C28 H60 Br P 0.045 g : 0.5 ml CDCl3
    tributylhexadecylphosphonium bromide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.47 B 1.65 to 1.38 C 1.26 D 0.97 E 0.93

         Hz     ppm     Int.
    

        231.38   2.584     42
        229.31   2.561     32
        229.00   2.557     33
        227.25   2.538     36
        226.25   2.527     37
        224.50   2.507     40
        224.13   2.503     40
        223.25   2.493     41
        222.81   2.488     42
        222.25   2.482     42
        221.94   2.479     42
        220.38   2.461     47
        219.94   2.456     46
        218.38   2.439     44
        216.63   2.419     38
        216.06   2.413     38
        215.56   2.407     39
        215.00   2.401     38
        213.31   2.382     34
        212.63   2.375     33
        212.50   2.373     33
        212.00   2.368     33
        211.69   2.364     33
        211.38   2.361     32
        210.38   2.350     30
        209.69   2.342     30
        209.25   2.337     30
        207.50   2.317     33
        206.94   2.311     32
        150.19   1.677     32
        149.81   1.673     32
        142.50   1.592    105
        138.94   1.552    113
        138.50   1.547    113
        137.13   1.532    105
        134.88   1.507    130
        132.19   1.476     94
        129.44   1.446     70
        129.13   1.442     68
        127.63   1.426     72
        124.13   1.386     48
        123.44   1.379     47
        123.13   1.375     46
        112.69   1.259   1000
         94.00   1.050     80
         93.81   1.048     80
         92.06   1.028     63
         91.88   1.026     63
         87.81   0.981    189
         84.81   0.947     82
         84.50   0.944     82
         82.44   0.921     76
         82.00   0.916     77
         81.63   0.912     77
         78.81   0.880     93
    

in CDCl3



KBr disc



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