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网站主页CAS数据库列表 142817-71-8更多图谱2,4,6-TRIS(1-CHLOROETHYL)-1,3,5-TRIOXANE(142817-71-8)质谱(MS)

2,4,6-TRIS(1-CHLOROETHYL)-1,3,5-TRIOXANE

产品名称 2,4,6-TRIS(1-CHLOROETHYL)-1,3,5-TRIOXANE

CAS号142817-71-8

分子式C9H15Cl3O3

分子量277.57


  • Mass

    MS-KW-0512          
    2,4,6-tris(1-chloroethyl)-1,3,5-trioxane
    C9H15Cl3O3          (Mass of molecular ion:    276)
    

       Source Temperature: 140 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          26.0       2.2
          27.0      12.2
          28.0      10.7
          29.0      25.9
          39.0       1.3
          41.0       1.2
          55.0       1.1
          56.0       4.3
          57.0      20.0
          58.0       2.1
          63.0       8.1
          64.0       4.4
          65.0       3.0
          66.0       1.4
          91.0       5.3
          92.0       6.0
          93.0     100.0
          94.0       5.4
          95.0      31.6
          96.0       1.0
         183.0       1.5
         185.0      10.5
         187.0       6.3
         189.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9H15Cl3O3 0.038 g : 0.5 ml CDCl3
    2,4,6-tris(1-chloroethyl)-1,3,5-trioxane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.984 B 4.025 C 1.537

         Hz     ppm     Int.
    

       1995.00   4.991    414
       1993.54   4.987     84
       1992.68   4.985     77
       1990.61   4.980    402
       1989.14   4.976     72
       1988.29   4.974     59
       1911.02   4.781      4
       1906.87   4.770      4
       1621.34   4.056     49
       1616.95   4.045     62
       1614.51   4.039    146
       1612.31   4.033     40
       1610.23   4.028    157
       1607.79   4.022    151
       1605.47   4.016     39
       1603.40   4.011    148
       1600.96   4.005     52
       1599.61   4.002     29
       1596.68   3.994     47
       1592.78   3.985      8
        839.73   2.101      5
        681.40   1.705      8
        674.57   1.688      8
        632.21   1.582     49
        617.19   1.544   1000
        610.36   1.527    956
        551.52   1.380      8
        544.68   1.363      8
    

in CDCl3



KBr disk



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