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MS-NW-0845 bis(2-chloroethyl) ether C4H8Cl2O (Mass of molecular ion: 142)
Source Temperature: 280 °C Sample Temperature: 150 °C Reservoir, 75 eV
14.0 1.0 15.0 1.9 26.0 3.3 27.0 47.3 28.0 35.5 29.0 4.6 31.0 9.8 32.0 8.2 36.0 1.1 42.0 1.0 43.0 3.1 44.0 1.0 45.0 2.4 49.0 4.6 51.0 1.5 61.0 1.0 62.0 2.2 63.0 73.2 64.0 2.2 65.0 23.6 93.0 100.0 94.0 3.3 95.0 31.8 96.0 1.1 106.0 1.5 142.0 1.7 144.0 1.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C4 H8 Cl2 O 0.05 ml : 0.5 ml CDCl3 bis(2-chloroethyl) ether Assign. Shift(ppm)
A *1 3.77 B *1 3.66
Hz ppm Int.
356.06 3.976 30 355.44 3.969 31 353.31 3.945 39 352.94 3.941 40 352.44 3.936 43 351.81 3.929 45 350.75 3.917 52 344.13 3.843 271 339.06 3.786 805 335.00 3.741 993 330.88 3.695 1000 326.88 3.650 851 321.88 3.595 301 310.94 3.472 41 310.06 3.463 36 309.44 3.456 36 308.88 3.449 36 308.56 3.446 34
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