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MS-NW-1046 tetrahydropyran C5H10O (Mass of molecular ion: 86)
Source Temperature: 250 °C Sample Temperature: 130 °C Reservoir, 75 eV
15.0 2.1 18.0 2.6 26.0 4.3 27.0 19.9 28.0 43.6 29.0 23.5 30.0 2.9 31.0 4.3 38.0 1.3 39.0 15.4 40.0 5.7 41.0 100.0 42.0 4.4 43.0 6.8 44.0 1.8 45.0 64.4 46.0 1.4 50.0 1.1 51.0 1.5 53.0 3.0 54.0 2.6 55.0 21.7 56.0 64.4 57.0 8.7 58.0 2.2 67.0 4.8 71.0 2.7 85.0 54.6 86.0 49.4 87.0 2.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H10 O 0.02 ml : 0.5 ml CDCl3 tetrahydropyran Assign. Shift(ppm)
A 3.65 B 1.59
Hz ppm Int.
331.75 3.705 410 329.56 3.680 323 329.19 3.676 333 326.75 3.649 655 324.56 3.624 429 324.19 3.620 437 322.63 3.603 358 321.63 3.592 270 146.44 1.636 871 145.63 1.627 806 144.88 1.618 898 143.38 1.601 1000 141.69 1.583 773 138.88 1.551 383 136.00 1.519 232
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