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1,2,3,4-四氢异喹啉 盐酸盐

产品名称 1,2,3,4-四氢异喹啉 盐酸盐

CAS号14099-81-1

分子式C9H12ClN

分子量169.65

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  • Mass

    MS-IW-8681          
    1,2,3,4-tetrahydroisoquinoline hydrochloride
    C9H11N HCl          (Mass of molecular ion:    133)
    

       Source Temperature: 170 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          18.0       1.9
          27.0       1.4
          28.0       2.5
          35.0       1.8
          36.0      21.6
          38.0       7.2
          39.0       3.0
          42.0       1.3
          50.0       2.7
          51.0       7.1
          52.0       2.4
          53.0       1.0
          63.0       2.8
          64.0       1.2
          64.5       6.7
          65.0       6.6
          65.5       7.4
          66.0       2.5
          66.5       1.7
          74.0       1.4
          75.0       1.7
          76.0       2.3
          77.0      14.1
          78.0      15.6
          79.0       3.7
          89.0       1.9
          90.0       2.3
          91.0       2.8
         101.0       1.2
         102.0       5.3
         103.0      21.6
         104.0      95.8
         105.0      21.6
         106.0       1.7
         115.0       4.9
         116.0       1.1
         117.0      11.9
         118.0       1.9
         128.0       2.1
         129.0       7.3
         130.0      15.7
         131.0       5.6
         132.0     100.0
         133.0      56.4
         134.0       5.5
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C9 H11 N 0.040 g : 0.5 ml DMSO-d6
    1,2,3,4-tetrahydroisoquinoline hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.94 B 7.22 C 4.21 D 3.30 E 3.011

         Hz     ppm     Int.
    

       3972.32   9.940    187
       2904.66   7.269     34
       2901.46   7.261     62
       2898.56   7.253    103
       2895.36   7.245    205
       2893.22   7.240    275
       2889.10   7.230    751
       2887.27   7.225   1000
       2885.13   7.220    596
       2883.30   7.215    586
       2879.18   7.205    308
       2874.60   7.193    139
       2873.69   7.191    147
       1682.89   4.211    503
       1320.34   3.304    307
       1315.00   3.291    198
       1209.72   3.027    290
       1203.46   3.012    507
       1197.20   2.996    238
    

in DMSO-d6



KBr disc



nujol mull