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MassMS-NW-5481 1-ethyl-3-piperidinol C7H15NO (Mass of molecular ion: 129)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 3.9 18.0 1.7 26.0 1.2 27.0 9.9 28.0 10.4 29.0 8.5 30.0 11.2 31.0 1.8 39.0 4.3 40.0 1.1 41.0 10.2 42.0 42.9 43.0 11.6 44.0 18.4 45.0 1.0 53.0 1.5 54.0 2.6 55.0 4.8 56.0 10.0 57.0 37.7 58.0 14.9 67.0 1.6 68.0 2.2 69.0 1.4 70.0 5.4 71.0 6.8 72.0 31.8 73.0 1.8 80.0 1.4 82.0 2.6 84.0 8.2 85.0 3.2 86.0 5.3 96.0 4.6 98.0 4.0 100.0 5.8 108.0 1.2 110.0 2.7 111.0 1.6 112.0 1.9 114.0 100.0 115.0 7.5 128.0 10.4 129.0 22.9 130.0 2.1
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C7 H15 N O 0.05 ml : 0.5 ml CDCl3 1-ethyl-3-piperidinol 
Assign. Shift(ppm)
A 4.06 B 3.763 C 2.701 D 2.50 E 2.414 F 2.20 to 2.120 G 1.80 to 1.730 J 1.548 K 1.384 L 1.070 90MHZ. : HSP-03-349 ASSIGNED BY COSY.
Hz ppm Int.1514.04 3.789 31 1510.74 3.781 53 1506.35 3.770 66 1502.93 3.761 91 1499.39 3.752 62 1495.12 3.742 49 1084.59 2.714 41 1083.98 2.713 41 1080.81 2.705 38 1080.44 2.704 37 1080.08 2.703 37 1075.93 2.693 42 1075.44 2.691 43 1074.10 2.688 42 1005.25 2.516 39 1005.00 2.515 39 1004.03 2.513 40 1002.56 2.509 41 1002.08 2.508 41 999.88 2.502 43 999.39 2.501 43 998.29 2.498 44 997.92 2.497 44 996.95 2.495 43 996.58 2.494 43 995.00 2.490 44 994.63 2.489 44 993.90 2.487 45 988.89 2.475 36 981.69 2.457 32 976.56 2.444 96 974.98 2.440 102 969.24 2.426 269 967.77 2.422 281 962.04 2.408 270 960.69 2.404 285 954.71 2.389 97 953.49 2.386 105 879.03 2.200 36 869.14 2.175 59 867.80 2.172 59 866.58 2.169 59 865.84 2.167 59 865.48 2.166 59 864.75 2.164 58 864.38 2.163 58 863.77 2.162 58 863.40 2.161 58 862.43 2.158 58 861.57 2.156 58 860.72 2.154 58 859.74 2.152 57 859.25 2.151 57 858.28 2.148 56 714.11 1.787 60 711.18 1.780 96 708.62 1.774 96 705.44 1.766 87 701.90 1.757 109 698.85 1.749 103 696.04 1.742 83 692.75 1.734 51 689.45 1.726 30 629.27 1.575 35 623.78 1.561 66 620.12 1.552 62 614.75 1.539 67 611.08 1.530 53 605.47 1.516 30 564.94 1.414 31 564.58 1.413 31 556.15 1.392 50 551.64 1.381 35 550.42 1.378 36 547.97 1.372 42 440.92 1.104 31 434.81 1.088 539 431.40 1.080 55 427.61 1.070 1000 420.29 1.052 468
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1H NMR 89.56 MHz C7 H15 N O 0.04 ml : 0.5 ml CDCl3 1-ethyl-3-piperidinol Assign. Shift(ppm)
A 3.78 B 3.57 C 2.624 D 2.40 E 2.42 to 2.17 F 1.88 to 1.27 G 1.064 J(A,C)=3.0HZ. 400MHZ. HSP-40-467.
Hz ppm Int.343.38 3.835 30 341.38 3.812 47 340.38 3.801 45 338.19 3.777 65 336.44 3.757 48 334.88 3.740 51 331.00 3.696 48 320.00 3.574 199 243.88 2.724 51 240.88 2.690 53 233.00 2.602 95 229.88 2.567 105 227.31 2.539 120 226.75 2.532 119 225.19 2.515 39 224.44 2.507 35 219.63 2.453 455 215.25 2.404 88 214.56 2.396 86 212.44 2.373 576 209.56 2.340 119 207.00 2.312 168 205.69 2.297 230 205.31 2.293 224 200.06 2.234 148 196.31 2.192 83 193.75 2.164 37 193.13 2.157 36 192.56 2.151 36 192.19 2.146 35 189.13 2.112 75 167.00 1.865 34 163.75 1.829 47 161.13 1.800 65 160.69 1.795 63 158.19 1.767 101 155.06 1.732 73 152.69 1.705 137 150.75 1.684 131 149.50 1.670 116 145.81 1.629 108 144.13 1.610 84 143.81 1.606 84 141.44 1.580 77 139.88 1.562 91 137.88 1.540 84 136.50 1.525 79 135.13 1.509 74 132.56 1.481 65 128.13 1.431 60 126.50 1.413 53 124.94 1.396 35 124.63 1.392 35 123.81 1.383 30 121.31 1.355 47 102.31 1.143 481 95.38 1.065 1000 91.81 1.026 35 90.94 1.016 39 88.00 0.983 364
in CDCl3
liquid film
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