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MassMS-NW-7560 1-ethyl-4-piperidinol C7H15NO (Mass of molecular ion: 129)
Source Temperature: 260 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 2.9 18.0 1.5 26.0 1.1 27.0 8.9 28.0 11.9 29.0 9.5 30.0 7.2 31.0 2.1 39.0 2.3 41.0 5.6 42.0 30.7 43.0 5.3 44.0 49.6 45.0 2.2 53.0 3.1 54.0 2.9 55.0 9.7 56.0 13.8 57.0 21.0 58.0 11.5 68.0 1.4 69.0 1.3 70.0 5.2 71.0 4.5 72.0 2.7 82.0 1.4 84.0 17.9 85.0 2.1 96.0 3.5 100.0 1.1 110.0 5.4 112.0 7.8 114.0 100.0 115.0 7.6 128.0 12.6 129.0 23.4 130.0 2.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H15 N O 0.05 ml : 0.5 ml CDCl3 1-ethyl-4-piperidinol 
Assign. Shift(ppm)
A 4.08 B 3.609 C 2.794 D 2.392 E 2.089 F 1.878 G 1.599 J 1.077
Hz ppm Int.1467.90 3.673 30 1467.41 3.672 30 1463.99 3.664 46 1459.35 3.652 61 1454.96 3.641 73 1450.68 3.630 57 1447.51 3.622 37 1445.92 3.618 41 1122.07 2.808 109 1116.09 2.793 103 1115.60 2.792 103 1110.84 2.780 112 1110.60 2.779 112 970.09 2.428 37 967.16 2.421 161 962.89 2.410 55 959.84 2.402 480 952.64 2.384 494 945.43 2.366 169 844.97 2.115 78 844.73 2.114 78 834.72 2.089 123 824.71 2.064 72 824.46 2.063 72 761.23 1.905 62 757.81 1.897 110 753.91 1.887 113 750.24 1.878 98 748.54 1.873 104 744.87 1.864 133 740.97 1.855 127 656.13 1.642 75 652.47 1.633 79 646.12 1.617 110 643.07 1.610 154 639.65 1.601 84 636.72 1.594 83 633.18 1.585 138 630.25 1.578 91 623.78 1.561 55 620.12 1.552 50 440.80 1.103 76 437.74 1.096 527 430.54 1.078 1000 423.22 1.059 511 420.41 1.052 68
in CDCl3
liquid film
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