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网站主页CAS数据库列表 13380-94-4更多图谱三环[5,2,1,0(2,6)]癸-8-酮(13380-94-4)质谱(MS)

三环[5,2,1,0(2,6)]癸-8-酮

产品名称 三环[5,2,1,0(2,6)]癸-8-酮

CAS号13380-94-4

分子式C10H14O

分子量150.22

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  • Mass

    MS-IW-0072          
    tricyclo(5.2.1.0(2,6))decane-8-one
    C10H14O             (Mass of molecular ion:    150)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0      12.6
          28.0       2.0
          29.0       3.7
          38.0       1.3
          39.0      22.8
          40.0       5.7
          41.0      20.9
          42.0       2.1
          43.0       1.9
          50.0       2.0
          51.0       6.4
          52.0       4.0
          53.0      14.4
          54.0      14.5
          55.0       9.6
          63.0       1.9
          65.0       8.4
          66.0      17.8
          67.0      37.2
          68.0      13.6
          69.0       1.8
          70.0       1.1
          77.0      19.6
          78.0      13.1
          79.0      85.1
          80.0      53.9
          81.0      39.9
          82.0      10.4
          83.0       3.9
          84.0       1.8
          85.0       2.1
          91.0      22.2
          92.0       8.3
          93.0      38.6
          94.0      16.3
          95.0       6.7
          96.0       2.1
         103.0       1.2
         104.0       5.3
         105.0       5.8
         106.0     100.0
         107.0      42.3
         108.0      24.5
         109.0      47.8
         110.0       3.9
         117.0       5.6
         119.0      10.9
         120.0       2.7
         121.0      31.0
         122.0      14.8
         123.0       1.7
         131.0       1.3
         132.0       5.1
         133.0       2.0
         134.0       2.0
         135.0       5.5
         148.0       3.0
         149.0       4.9
         150.0      78.2
         151.0       9.3
         152.0       1.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H14 O 0.05 ml : 0.5 ml CDCl3
    tricyclo(5.2.1.0(2,6))decane-8-one
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 2.403 B 2.360 C *1 2.12 D 2.021 E 1.98 F 1.78 G 1.77 to 1.75 J 1.529 K 1.347 L 1.09 ASSIGNED BY C-H COSY

         Hz     ppm     Int.
    

        963.26   2.411    451
        962.04   2.408    466
        958.86   2.400    480
        958.13   2.398    471
        957.64   2.397    472
        943.24   2.361   1000
        857.91   2.147    311
        852.29   2.133    417
        849.12   2.125    621
        845.70   2.117    456
        840.33   2.103    365
        831.42   2.081    118
        822.88   2.060    327
        818.36   2.048    319
        805.66   2.016    538
        801.27   2.005    487
        799.07   2.000    277
        797.61   1.996    309
        795.90   1.992    300
        794.43   1.988    249
        790.65   1.979    336
        789.06   1.975    357
        787.60   1.971    336
        786.25   1.968    305
        785.03   1.965    369
        783.69   1.961    368
        781.86   1.957    333
        777.95   1.947    235
        776.37   1.943    295
        774.90   1.939    283
        767.94   1.922    141
        723.14   1.810    620
        718.75   1.799    877
        715.33   1.790    311
        714.84   1.789    309
        709.11   1.775    557
        704.35   1.763    624
        701.54   1.756    817
        698.36   1.748    419
        696.17   1.742    347
        618.77   1.549    193
        617.31   1.545    470
        615.97   1.542    596
        614.50   1.538    413
        613.04   1.534    167
        609.74   1.526    133
        608.03   1.522    164
        606.57   1.518    330
        605.10   1.515    469
        603.64   1.511    365
        602.17   1.507    163
        564.45   1.413    106
        557.74   1.396    176
        551.88   1.381    300
        545.29   1.365    496
        539.43   1.350    365
        532.84   1.334    528
        526.37   1.318    288
        520.39   1.303    255
        517.21   1.295     31
        513.92   1.286    137
        457.89   1.146    136
        455.20   1.139     59
        450.93   1.129    264
        445.07   1.114    332
        443.36   1.110    300
        438.35   1.097    437
        437.26   1.095    410
        431.76   1.081    386
        430.66   1.078    428
        425.78   1.066    249
        423.95   1.061    322
        417.85   1.046    196
        413.94   1.036     54
        411.01   1.029     98
    

in CDCl3



liquid film