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MS-IW-6985 S,S'-(thiodi-p-phenylene) bis(2-methyl-2-propenethioate) C20H18O2S3 (Mass of molecular ion: 386)
Source Temperature: 170 °C Sample Temperature: 180 °C Direct, 75 eV
17.0 1.5 18.0 7.4 28.0 1.4 39.0 2.4 41.0 36.4 42.0 1.2 57.0 1.0 69.0 100.0 70.0 5.5 71.0 1.0 108.0 1.0 171.0 1.0 317.0 2.5 318.0 1.8 358.0 1.2 386.0 47.2 387.0 11.5 388.0 7.8 389.0 1.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C20 H18 O2 S3 0.042 g : 0.5 ml CDCl3 S,S'-(thiodi-p-phenylene) bis(2-methyl-2-propenethioate) Assign. Shift(ppm)
A *1 7.385 B *1 7.371 C 6.202 D 5.709 E 2.004
Hz ppm Int.
2958.50 7.403 120 2957.52 7.401 89 2955.69 7.396 78 2952.39 7.388 136 2949.71 7.381 1000 2947.27 7.375 913 2944.58 7.368 95 2941.28 7.360 70 2939.45 7.356 88 2938.48 7.353 110 2479.37 6.204 348 2478.39 6.202 348 2284.18 5.716 119 2282.59 5.712 311 2281.13 5.708 308 2279.54 5.704 114 802.12 2.008 713 801.15 2.005 859 800.54 2.004 824 799.68 2.001 654
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