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MS-IW-4932 4,4'-thiodibenzenethiol C12H10S3 (Mass of molecular ion: 250)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
28.0 5.3 32.0 1.9 39.0 1.9 45.0 2.6 63.0 2.6 65.0 4.1 69.0 5.4 70.0 1.0 71.0 1.3 77.0 1.6 82.0 2.0 92.0 2.3 95.0 1.9 96.0 2.2 97.0 4.1 108.0 9.3 108.5 3.4 109.0 4.9 110.0 5.4 125.0 3.2 134.0 1.0 139.0 1.7 140.0 5.3 141.0 19.5 142.0 2.2 143.0 1.9 152.0 1.5 171.0 4.5 172.0 1.9 173.0 1.1 183.0 1.3 184.0 19.0 185.0 5.6 186.0 5.2 205.0 1.2 215.0 2.2 216.0 5.6 217.0 16.2 218.0 5.0 219.0 2.0 249.0 14.6 250.0 100.0 251.0 17.2 252.0 14.8 253.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H10 S3 0.038 g : 0.5 ml CDCl3 4,4'-thiodibenzenethiol Assign. Shift(ppm)
A 7.18 B 3.46
Hz ppm Int.
2878.54 7.203 34 2877.32 7.200 29 2875.00 7.194 34 2872.68 7.188 58 2869.38 7.180 1000 2868.90 7.179 973 2865.48 7.170 44 2865.23 7.170 44 2863.16 7.165 34 2860.72 7.159 33 2859.74 7.156 38 1380.74 3.455 531
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