图谱信息 供应商 相关产品
网站主页CAS数据库列表 1271-86-9更多图谱N,N-二甲氨基甲基二茂铁(1271-86-9)质谱(MS)

N,N-二甲氨基甲基二茂铁

产品名称 N,N-二甲氨基甲基二茂铁

CAS号1271-86-9

分子式C13H17FeN10*

分子量243.13

展开


  • Mass

    MS-NW-2186          
    (dimethylaminomethyl)ferrocene
    C13H17FeN           (Mass of molecular ion:    243)
    

       Source Temperature: 280 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       2.1
          17.0       1.0
          18.0       4.8
          28.0       1.3
          30.0       2.2
          39.0       4.0
          41.0       1.0
          42.0       9.1
          43.0       2.1
          44.0       7.5
          45.0       2.4
          51.0       1.8
          52.0       1.7
          54.0       1.6
          56.0      25.5
          57.0       2.6
          58.0      11.3
          65.0       2.0
          66.0       1.6
          72.0       1.1
          77.0       3.8
          78.0       5.5
          79.0       4.1
          81.0       3.3
          83.0       1.9
          94.0       2.2
          95.0       3.6
          97.0       2.7
          99.0       3.8
         100.0       1.0
         106.0       2.0
         119.0       3.6
         120.0       2.4
         121.0      50.1
         122.0       7.2
         128.0       1.0
         129.0       1.5
         134.0       8.7
         135.0       6.1
         148.0       1.6
         160.0       1.3
         161.0       2.3
         162.0      16.7
         163.0      14.6
         164.0       2.9
         165.0       1.3
         175.0       5.0
         176.0       1.1
         177.0       5.8
         178.0       4.0
         184.0       1.8
         186.0      23.0
         187.0       3.4
         197.0       6.6
         198.0       2.1
         199.0     100.0
         200.0      30.5
         201.0       3.6
         214.0       1.7
         227.0       2.7
         228.0       1.8
         240.0       1.4
         241.0       6.5
         242.0      17.2
         243.0      98.4
         244.0      16.6
         245.0       1.4
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C13 H17 Fe N 0.04 ml : 0.5 ml CDCl3
    (dimethylaminomethyl)ferrocene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.12 B 3.276 C 2.162

         Hz     ppm     Int.
    

        374.25   4.179     30
        372.63   4.161     75
        372.50   4.160     75
        371.06   4.144    120
        368.69   4.117    139
        367.31   4.102   1000
        362.94   4.053     30
        293.38   3.276    157
        193.63   2.163    621
    

CCl4 solution



liquid film