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MassMS-NW-0616 p-anilinophenol C12H11NO (Mass of molecular ion: 185)
Source Temperature: 170 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 1.9 27.0 2.6 28.0 2.0 38.0 1.3 39.0 7.4 50.0 2.1 51.0 7.1 52.0 3.8 53.0 3.4 54.0 1.0 55.0 1.3 63.0 2.6 64.0 1.7 65.0 5.9 66.0 6.2 77.0 7.3 78.0 3.2 79.0 1.1 80.0 1.5 81.0 4.3 82.0 3.2 83.5 1.4 91.0 1.2 92.5 1.0 93.0 1.9 103.0 1.8 104.0 1.4 108.0 3.4 115.0 1.7 117.0 1.2 120.0 1.1 127.0 1.9 128.0 4.2 129.0 4.7 130.0 4.0 131.0 1.0 139.0 1.0 140.0 1.0 154.0 4.2 155.0 1.7 156.0 7.2 157.0 1.7 158.0 1.1 166.0 3.4 167.0 3.5 168.0 2.2 170.0 1.1 183.0 4.5 184.0 14.5 185.0 100.0 186.0 13.4 187.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H11 N O 0.040 g : 0.5 ml CDCl3 p-anilinophenol 
Assign. Shift(ppm)
A 7.197 B 6.975 C 6.878 D 6.829 E 6.749 F 5.4
Hz ppm Int.2884.40 7.218 501 2882.81 7.214 254 2876.95 7.199 789 2875.98 7.197 802 2868.53 7.178 609 2792.60 6.988 839 2790.65 6.983 366 2783.81 6.966 1000 2780.64 6.958 173 2752.56 6.888 783 2744.87 6.869 693 2736.33 6.847 271 2729.00 6.829 437 2721.68 6.811 215 2701.29 6.760 811 2692.63 6.738 680 2144.41 5.366 77
in CDCl3
CCl4 solution
KBr disc
nujol mull
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