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MS-NW-8523 (methylamino)acetaldehyde dimethyl acetal C5H13NO2 (Mass of molecular ion: 119)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
15.0 11.9 18.0 5.5 27.0 2.9 28.0 25.8 29.0 9.5 30.0 5.9 31.0 12.6 32.0 1.0 41.0 2.3 42.0 12.3 43.0 7.1 44.0 100.0 45.0 14.0 47.0 24.7 56.0 22.5 57.0 5.4 58.0 16.1 59.0 4.6 72.0 3.7 73.0 1.8 75.0 97.7 76.0 3.4 86.0 1.5 88.0 28.9 89.0 8.7 119.0 1.9
parameter in CDCl3
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1H NMR 300 MHz C5 H13 N O2 0.04 ml : 0.5 ml CDCl3 (methylamino)acetaldehyde dimethyl acetal Parameter ppm Hz
D(A) 4.462 D(B) 2.701 J(A,B) 5.48 D(C) 3.387 D(D) 2.454 D(E) 1.25
Hz ppm Int.
1344.10 4.480 41 1338.62 4.462 83 1333.17 4.444 43 1016.08 3.387 1000 813.04 2.710 169 807.56 2.692 166 736.21 2.454 500 375.01 1.250 167
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