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MS-NW-0585 N,N-dimethyl-m-toluidine C9H13N (Mass of molecular ion: 135)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 2.0 27.0 1.3 39.0 4.5 41.0 1.5 42.0 5.0 44.0 2.2 50.0 1.2 51.0 3.1 52.0 1.3 58.5 1.0 63.0 2.8 64.0 1.0 65.0 7.1 66.5 4.6 67.5 2.0 77.0 4.8 78.0 1.7 79.0 1.5 89.0 2.0 90.0 1.2 91.0 15.6 92.0 3.4 93.0 1.9 104.0 1.0 105.0 2.1 106.0 1.3 118.0 8.3 119.0 10.3 120.0 6.2 121.0 1.9 132.0 1.3 133.0 1.1 134.0 100.0 135.0 82.5 136.0 8.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H13 N 10.7 mol% in CDCl3 N,N-dimethyl-m-toluidine Assign. Shift(ppm)
A 6.46 to 6.62 B 7.088 C 2.88 D 2.30
Hz ppm Int.
635.88 7.101 31 628.75 7.021 37 589.44 6.582 122 588.94 6.576 113 586.69 6.551 37 585.94 6.543 36 585.19 6.535 31 583.00 6.510 66 258.06 2.882 1000 255.75 2.856 54 206.31 2.304 274 205.69 2.297 256
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