(1,5-环辛二烯)二氯化铂(II)

产品名称 (1,5-环辛二烯)二氯化铂(II)

CAS号12080-32-9

分子式C8H12Cl2Pt

分子量374.16

¹³CNMR

Mass

MS-IW-1341          
(1,5-cyclooctadiene)platinum(II) chloride
C8H12Cl2Pt          (Mass of molecular ion:    373)

   Source Temperature: 190 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      18.0       2.6
      27.0      10.0
      28.0       3.6
      29.0       1.8
      35.0       3.5
      36.0      28.7
      37.0       1.3
      38.0      10.2
      39.0      36.2
      40.0       3.0
      41.0      18.3
      50.0       4.7
      51.0      10.3
      52.0       5.6
      53.0      13.1
      54.0      93.9
      55.0       6.0
      62.0       1.2
      63.0       3.2
      65.0      14.3
      66.0      23.6
      67.0     100.0
      68.0       6.4
      74.0       1.3
      77.0      24.6
      78.0      17.2
      79.0      58.2
      80.0      67.6
      81.0       5.1
      91.0      21.6
      92.0       2.4
      93.0      21.0
      94.0       1.7
     102.0       1.9
     103.0       4.6
     104.0       3.0
     105.0       8.1
     106.0       2.8
     107.0       3.0
     108.0      10.8
     109.0       1.1
     148.0       1.7
     148.5       1.7
     149.0       3.8
     149.5       2.8
     150.0       2.9
     151.0       1.1
     220.0       2.2
     221.0       3.5
     222.0       2.7
     223.0       1.1
     231.0       1.6
     232.0       2.7
     233.0       3.9
     234.0       2.9
     235.0       2.1
     243.0       1.0
     244.0       2.5
     245.0       4.3
     246.0       4.9
     247.0       4.6
     248.0       3.1
     249.0       1.8
     258.0       1.1
     259.0       2.1
     260.0       2.1
     261.0       1.4
     269.0       2.0
     270.0       5.1
     271.0       7.3
     272.0      10.9
     273.0       9.9
     274.0       7.1
     275.0       2.5
     276.0       1.6
     283.0       1.2
     284.0       2.4
     285.0       2.7
     286.0       1.7
     295.0       5.2
     296.0      15.8
     297.0      23.6
     298.0      32.2
     299.0      32.5
     300.0      41.6
     301.0      47.9
     302.0      39.5
     303.0      19.1
     304.0       5.8
     305.0       4.5
     334.0       1.7
     335.0       1.4
     336.0      13.3
     337.0      30.3
     338.0      33.1
     339.0      24.6
     340.0      13.3
     341.0       8.8
     342.0       1.6
     343.0       1.3
     372.0      29.3
     373.0      32.5
     374.0      43.7
     375.0      23.1
     376.0      25.6
     377.0       5.4
     378.0       6.9

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₈ H₁₂ Cl₂ Pt	0.032 g : 0.5 ml DMSO-d₆
(1,5-cyclooctadiene)platinum(II) chloride

    Assign.     Shift(ppm)

      A             5.49
      B     *1      2.61
      C     *1      2.25

     Hz     ppm     Int.

   2231.93   5.585    180
   2211.06   5.533     64
   2209.23   5.528    110
   2208.86   5.527    112
   2208.37   5.526    114
   2207.28   5.524    118
   2199.58   5.504    971
   2198.24   5.501    971
   2197.14   5.498    989
   2189.33   5.479    138
   2189.09   5.478    138
   2188.72   5.477    138
   2188.11   5.476    142
   2187.74   5.475    144
   2187.26   5.473    144
   2184.33   5.466     66
   2164.79   5.417    184
   1066.77   2.670     64
   1064.82   2.665     98
   1062.87   2.660    101
   1061.52   2.657    125
   1061.16   2.656    123
   1060.18   2.653    110
   1055.30   2.641    241
   1053.96   2.638    256
   1051.03   2.630    486
   1048.71   2.625    621
   1048.22   2.623    606
   1046.14   2.618    610
   1045.17   2.616    599
   1043.33   2.611    602
   1041.87   2.607    654
   1040.53   2.604    661
   1039.79   2.602    641
   1036.87   2.595    702
   1031.49   2.581    308
   1030.40   2.579    297
   1025.27   2.566    166
   1025.02   2.565    166
   1022.46   2.559    110
   1022.09   2.558    109
   1021.48   2.556    107
   1020.14   2.553     85
   1019.78   2.552     81
   1019.04   2.550     74
   1018.07   2.548     74
   1017.58   2.547     74
   1017.21   2.546     72
   1016.72   2.545     68
   1016.48   2.544     68
   1015.87   2.542     70
   1015.63   2.542     70
   1015.38   2.541     70
    934.69   2.339     66
    934.45   2.339     66
    929.57   2.326    168
    927.98   2.322    177
    926.15   2.318    144
    925.29   2.316    129
    924.32   2.313    134
    923.95   2.312    133
    923.22   2.311    138
    920.90   2.305    171
    920.41   2.304    173
    919.80   2.302    171
    918.95   2.300    168
    918.58   2.299    166
    918.21   2.298    160
    917.97   2.297    160
    917.60   2.297    157
    917.11   2.295    151
    916.38   2.293    166
    915.41   2.291    169
    915.04   2.290    169
    912.60   2.284    326
    904.66   2.264    969
    896.61   2.244   1000
    888.43   2.224    285
    885.99   2.217    166
    885.62   2.216    166
    884.89   2.215    168
    884.40   2.213    162
    883.79   2.212    162
    883.42   2.211    160
    882.69   2.209    164
    881.96   2.207    166
    880.86   2.205    168
    880.49   2.204    162
    880.25   2.203    162
    877.32   2.196    109
    875.98   2.192    101
    875.61   2.191    101
    875.24   2.191    103
    874.02   2.187    118
    873.29   2.186    127
    872.68   2.184    131
    871.95   2.182    123
    870.00   2.177     88

in DMSO-d6

KBr disc

nujol mull

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