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MassMS-IW-1341 (1,5-cyclooctadiene)platinum(II) chloride C8H12Cl2Pt (Mass of molecular ion: 373)
Source Temperature: 190 °C Sample Temperature: 130 °C Direct, 75 eV
18.0 2.6 27.0 10.0 28.0 3.6 29.0 1.8 35.0 3.5 36.0 28.7 37.0 1.3 38.0 10.2 39.0 36.2 40.0 3.0 41.0 18.3 50.0 4.7 51.0 10.3 52.0 5.6 53.0 13.1 54.0 93.9 55.0 6.0 62.0 1.2 63.0 3.2 65.0 14.3 66.0 23.6 67.0 100.0 68.0 6.4 74.0 1.3 77.0 24.6 78.0 17.2 79.0 58.2 80.0 67.6 81.0 5.1 91.0 21.6 92.0 2.4 93.0 21.0 94.0 1.7 102.0 1.9 103.0 4.6 104.0 3.0 105.0 8.1 106.0 2.8 107.0 3.0 108.0 10.8 109.0 1.1 148.0 1.7 148.5 1.7 149.0 3.8 149.5 2.8 150.0 2.9 151.0 1.1 220.0 2.2 221.0 3.5 222.0 2.7 223.0 1.1 231.0 1.6 232.0 2.7 233.0 3.9 234.0 2.9 235.0 2.1 243.0 1.0 244.0 2.5 245.0 4.3 246.0 4.9 247.0 4.6 248.0 3.1 249.0 1.8 258.0 1.1 259.0 2.1 260.0 2.1 261.0 1.4 269.0 2.0 270.0 5.1 271.0 7.3 272.0 10.9 273.0 9.9 274.0 7.1 275.0 2.5 276.0 1.6 283.0 1.2 284.0 2.4 285.0 2.7 286.0 1.7 295.0 5.2 296.0 15.8 297.0 23.6 298.0 32.2 299.0 32.5 300.0 41.6 301.0 47.9 302.0 39.5 303.0 19.1 304.0 5.8 305.0 4.5 334.0 1.7 335.0 1.4 336.0 13.3 337.0 30.3 338.0 33.1 339.0 24.6 340.0 13.3 341.0 8.8 342.0 1.6 343.0 1.3 372.0 29.3 373.0 32.5 374.0 43.7 375.0 23.1 376.0 25.6 377.0 5.4 378.0 6.9
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C8 H12 Cl2 Pt 0.032 g : 0.5 ml DMSO-d6 (1,5-cyclooctadiene)platinum(II) chloride 
Assign. Shift(ppm)
A 5.49 B *1 2.61 C *1 2.25
Hz ppm Int.2231.93 5.585 180 2211.06 5.533 64 2209.23 5.528 110 2208.86 5.527 112 2208.37 5.526 114 2207.28 5.524 118 2199.58 5.504 971 2198.24 5.501 971 2197.14 5.498 989 2189.33 5.479 138 2189.09 5.478 138 2188.72 5.477 138 2188.11 5.476 142 2187.74 5.475 144 2187.26 5.473 144 2184.33 5.466 66 2164.79 5.417 184 1066.77 2.670 64 1064.82 2.665 98 1062.87 2.660 101 1061.52 2.657 125 1061.16 2.656 123 1060.18 2.653 110 1055.30 2.641 241 1053.96 2.638 256 1051.03 2.630 486 1048.71 2.625 621 1048.22 2.623 606 1046.14 2.618 610 1045.17 2.616 599 1043.33 2.611 602 1041.87 2.607 654 1040.53 2.604 661 1039.79 2.602 641 1036.87 2.595 702 1031.49 2.581 308 1030.40 2.579 297 1025.27 2.566 166 1025.02 2.565 166 1022.46 2.559 110 1022.09 2.558 109 1021.48 2.556 107 1020.14 2.553 85 1019.78 2.552 81 1019.04 2.550 74 1018.07 2.548 74 1017.58 2.547 74 1017.21 2.546 72 1016.72 2.545 68 1016.48 2.544 68 1015.87 2.542 70 1015.63 2.542 70 1015.38 2.541 70 934.69 2.339 66 934.45 2.339 66 929.57 2.326 168 927.98 2.322 177 926.15 2.318 144 925.29 2.316 129 924.32 2.313 134 923.95 2.312 133 923.22 2.311 138 920.90 2.305 171 920.41 2.304 173 919.80 2.302 171 918.95 2.300 168 918.58 2.299 166 918.21 2.298 160 917.97 2.297 160 917.60 2.297 157 917.11 2.295 151 916.38 2.293 166 915.41 2.291 169 915.04 2.290 169 912.60 2.284 326 904.66 2.264 969 896.61 2.244 1000 888.43 2.224 285 885.99 2.217 166 885.62 2.216 166 884.89 2.215 168 884.40 2.213 162 883.79 2.212 162 883.42 2.211 160 882.69 2.209 164 881.96 2.207 166 880.86 2.205 168 880.49 2.204 162 880.25 2.203 162 877.32 2.196 109 875.98 2.192 101 875.61 2.191 101 875.24 2.191 103 874.02 2.187 118 873.29 2.186 127 872.68 2.184 131 871.95 2.182 123 870.00 2.177 88
in DMSO-d6
KBr disc
nujol mull
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