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α,α,α-三联吡啶

产品名称 α,α,α-三联吡啶

CAS号1148-79-4

分子式C15H11N3

分子量233.27

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  • Mass

    MS-KW-0506          
    2,2':6',2''-terpyridine
    C15H11N3            (Mass of molecular ion:    233)
    

       Source Temperature: 150 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          50.0       1.4
          51.0       4.2
          52.0       1.9
          75.0       1.3
          76.0       2.0
          77.0       1.3
          78.0       9.0
          79.0       2.2
          89.0       1.2
         101.0       1.4
         102.0       1.8
         103.0       7.1
         103.5       1.8
         115.5       1.0
         116.5       9.2
         117.0       1.7
         128.0       3.8
         129.0       2.2
         130.0       1.6
         131.0       1.2
         155.0      10.9
         156.0       1.8
         205.0      14.0
         206.0       5.7
         207.0       3.6
         230.0       1.5
         231.0       2.5
         232.0      33.2
         233.0     100.0
         234.0      17.1
         235.0       1.4
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C15 H11 N3 0.042 g : 0.5 ml CDCl3
    2,2':6',2''-terpyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.68 B 8.61 C 8.45 D 7.93 E 7.83 F 7.30

         Hz     ppm     Int.
    

        781.69   8.729    269
        780.81   8.719    363
        779.88   8.708    338
        778.94   8.698    336
        776.94   8.676    284
        776.00   8.665    590
        775.63   8.661    589
        774.25   8.646    806
        773.38   8.636    291
        767.63   8.572    411
        766.63   8.560    585
        765.44   8.547    353
        761.44   8.503    589
        760.69   8.494    575
        753.44   8.413   1000
        717.88   8.016    432
        710.75   7.937    349
        709.38   7.921    496
        707.31   7.898    310
        702.25   7.842    406
        701.69   7.835    528
        699.75   7.814    483
        693.75   7.747    324
        691.88   7.726    322
        659.75   7.367    377
        658.44   7.352    371
        655.00   7.314    340
        653.69   7.299    356
        652.25   7.283    296
        650.94   7.269    343
        647.50   7.230    271
        646.25   7.216    241
    

in CDCl3



KBr disc



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