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MassMS-KW-0506 2,2':6',2''-terpyridine C15H11N3 (Mass of molecular ion: 233)
Source Temperature: 150 °C Sample Temperature: 100 °C Direct, 75 eV
50.0 1.4 51.0 4.2 52.0 1.9 75.0 1.3 76.0 2.0 77.0 1.3 78.0 9.0 79.0 2.2 89.0 1.2 101.0 1.4 102.0 1.8 103.0 7.1 103.5 1.8 115.5 1.0 116.5 9.2 117.0 1.7 128.0 3.8 129.0 2.2 130.0 1.6 131.0 1.2 155.0 10.9 156.0 1.8 205.0 14.0 206.0 5.7 207.0 3.6 230.0 1.5 231.0 2.5 232.0 33.2 233.0 100.0 234.0 17.1 235.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C15 H11 N3 0.042 g : 0.5 ml CDCl3 2,2':6',2''-terpyridine 
Assign. Shift(ppm)
A 8.68 B 8.61 C 8.45 D 7.93 E 7.83 F 7.30
Hz ppm Int.781.69 8.729 269 780.81 8.719 363 779.88 8.708 338 778.94 8.698 336 776.94 8.676 284 776.00 8.665 590 775.63 8.661 589 774.25 8.646 806 773.38 8.636 291 767.63 8.572 411 766.63 8.560 585 765.44 8.547 353 761.44 8.503 589 760.69 8.494 575 753.44 8.413 1000 717.88 8.016 432 710.75 7.937 349 709.38 7.921 496 707.31 7.898 310 702.25 7.842 406 701.69 7.835 528 699.75 7.814 483 693.75 7.747 324 691.88 7.726 322 659.75 7.367 377 658.44 7.352 371 655.00 7.314 340 653.69 7.299 356 652.25 7.283 296 650.94 7.269 343 647.50 7.230 271 646.25 7.216 241
in CDCl3
KBr disc
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