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MassMS-NW-4168 5,6,7,8-tetrahydro-2-naphthol C10H12O (Mass of molecular ion: 148)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 1.1 27.0 3.4 38.0 1.0 39.0 6.3 41.0 3.4 50.0 1.9 51.0 5.5 52.0 2.0 53.0 2.9 55.0 2.7 62.0 1.2 63.0 3.1 64.0 1.4 65.0 5.0 65.5 1.2 66.0 2.1 72.0 1.2 73.0 1.6 74.0 1.1 77.0 6.9 78.0 2.1 79.0 2.1 89.0 1.6 91.0 17.6 92.0 3.2 94.0 2.0 103.0 2.6 104.0 1.8 105.0 2.4 107.0 14.8 108.0 1.3 115.0 4.6 116.0 1.3 117.0 2.1 119.0 5.8 120.0 100.0 121.0 9.0 127.0 2.3 128.0 1.9 129.0 1.7 130.0 1.5 131.0 5.2 132.0 3.6 133.0 6.4 144.0 1.1 145.0 1.7 146.0 1.2 147.0 23.3 148.0 57.4 149.0 6.4
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C10 H12 O 0.049 g : 0.5 ml CDCl3 5,6,7,8-tetrahydro-2-naphthol 
Assign. Shift(ppm)
A 6.90 B 6.57 C 6.52 D 5.05 E 2.67 F 1.75
Hz ppm Int.622.88 6.955 165 622.00 6.946 115 615.75 6.876 178 614.25 6.859 231 593.81 6.631 189 591.06 6.600 307 583.94 6.521 723 451.94 5.047 1000 246.13 2.749 194 239.56 2.675 613 238.06 2.659 418 233.13 2.604 267 162.88 1.819 342 159.81 1.785 392 159.00 1.776 417 156.25 1.745 867 154.25 1.723 342 153.06 1.710 403 152.56 1.704 415 149.63 1.671 253
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1H NMR 399.65 MHz C10 H12 O 14.0 mg : 0.5 ml CDCl3 5,6,7,8-tetrahydro-2-naphthol Assign. Shift(ppm)
A 6.923 B 6.586 C 6.540 D 4.75 E 2.691 F 1.761
Hz ppm Int.2771.12 6.934 271 2762.82 6.914 299 2637.70 6.601 189 2635.01 6.594 225 2629.52 6.580 160 2626.71 6.573 214 2614.99 6.544 337 2614.62 6.543 346 2612.18 6.537 252 1898.44 4.751 316 1079.96 2.703 337 1076.66 2.695 294 1074.22 2.688 290 1073.49 2.687 291 1070.80 2.680 335 1064.58 2.664 136 716.19 1.793 49 713.99 1.787 66 709.72 1.776 378 706.42 1.768 514 703.13 1.760 1000 699.83 1.752 479 696.41 1.743 317 693.60 1.736 46 692.14 1.732 54 689.94 1.727 41
in CDCl3
KBr disc
nujol mull
4880 A,200 M,liquid
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