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MS-NW-0858 decanoyl chloride C10H19ClO (Mass of molecular ion: 190)
Source Temperature: 280 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 2.1 26.0 3.7 27.0 51.5 28.0 13.4 29.0 46.9 30.0 1.1 35.0 1.5 36.0 2.1 38.0 2.1 39.0 41.0 40.0 7.7 41.0 100.0 42.0 26.1 43.0 60.8 44.0 2.2 50.0 1.5 51.0 3.0 52.0 1.4 53.0 10.2 54.0 11.7 55.0 70.6 56.0 23.3 57.0 30.8 58.0 1.5 60.0 4.2 63.0 3.6 64.0 1.0 65.0 2.8 66.0 1.5 67.0 10.1 68.0 12.0 69.0 28.3 70.0 16.6 71.0 20.0 72.0 1.5 73.0 4.4 77.0 2.1 78.0 5.5 79.0 4.1 80.0 2.5 81.0 12.0 82.0 7.6 83.0 23.2 84.0 61.3 85.0 9.1 86.0 2.2 87.0 1.0 91.0 4.9 93.0 3.4 94.0 2.7 95.0 6.1 96.0 1.3 97.0 19.9 98.0 78.1 99.0 6.4 100.0 1.0 102.0 3.0 104.0 1.2 105.0 1.4 107.0 2.6 108.0 1.6 110.0 25.5 111.0 12.9 112.0 15.7 113.0 1.6 116.0 2.2 121.0 1.3 125.0 2.7 126.0 2.5 127.0 1.0 128.0 1.6 129.0 2.2 136.0 4.1 137.0 2.4 154.0 2.2 155.0 52.5 156.0 6.0 172.0 1.1 174.0 1.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H19 Cl O 0.04 ml : 0.5 ml CDCl3 decanoyl chloride Assign. Shift(ppm)
A 2.872 B 1.71 C 1.41 D 1.27 E 0.888
Hz ppm Int.
264.94 2.959 117 264.50 2.954 109 257.75 2.878 303 250.75 2.800 194 250.31 2.795 204 160.19 1.789 40 159.69 1.784 38 158.25 1.767 32 157.94 1.764 30 157.63 1.761 31 156.50 1.748 34 152.88 1.708 63 150.25 1.678 37 149.19 1.666 36 148.69 1.661 37 147.44 1.647 40 146.25 1.633 44 145.50 1.625 43 126.63 1.414 57 126.06 1.408 59 125.75 1.405 59 124.94 1.396 60 114.19 1.276 1000 105.13 1.174 34 84.00 0.938 93 82.06 0.917 75 81.94 0.915 75 81.56 0.911 75 81.13 0.906 73 79.00 0.883 323 75.25 0.841 42 72.94 0.815 63 71.88 0.803 48
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