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网站主页CAS数据库列表 111-19-3更多图谱癸二酰氯(111-19-3)核磁图(13CNMR)

癸二酰氯

产品名称 癸二酰氯

CAS号111-19-3

分子式C10H16Cl2O2

分子量239.14

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  • Mass

    MS-IW-3596          
    sebacoyl dichloride
    C10H16Cl2O2         (Mass of molecular ion:    238)
    

       Source Temperature: 220 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          27.0      15.0
          28.0       5.4
          29.0      11.1
          35.0       1.8
          36.0      14.1
          38.0       4.7
          39.0      13.1
          40.0       2.9
          41.0      44.3
          42.0      12.3
          43.0      14.1
          51.0       1.2
          53.0       5.3
          54.0       7.3
          55.0     100.0
          56.0      11.1
          57.0       5.6
          63.0       5.1
          65.0       2.0
          67.0      12.1
          68.0      11.8
          69.0      32.2
          70.0       7.8
          71.0       1.4
          77.0       2.5
          78.0       8.1
          79.0       8.1
          80.0      16.3
          81.0      13.1
          82.0       6.3
          83.0      19.0
          84.0      48.2
          85.0       3.1
          91.0       3.1
          93.0       3.9
          94.0       6.6
          95.0      11.0
          96.0       4.3
          97.0      15.9
          98.0      81.2
          99.0       5.5
         105.0       1.4
         107.0       8.1
         109.0       4.0
         110.0       6.0
         111.0       7.8
         112.0       4.2
         119.0       1.0
         120.0       1.1
         121.0       7.1
         122.0       2.4
         123.0       3.3
         124.0       2.8
         125.0      11.5
         126.0       1.0
         137.0       1.3
         138.0      10.4
         139.0      14.3
         140.0       1.3
         167.0      16.1
         168.0       1.8
         203.0      14.9
         204.0       1.6
         205.0       5.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H16 Cl2 O2 0.05 ml : 0.5 ml CDCl3
    sebacoyl dichloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.890 B 1.702 C 1.33

         Hz     ppm     Int.
    

       1162.72   2.910    574
       1155.40   2.892   1000
       1148.19   2.873    681
        695.92   1.742     54
        688.72   1.724    178
        681.27   1.705    285
        673.95   1.687    243
        666.75   1.669     97
        548.10   1.372    114
        546.26   1.367    111
        542.72   1.358    156
        529.66   1.326    677
    

in CDCl3



liquid film