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MassMS-NW-1454 3,3'-thiodipropionitrile C6H8N2S (Mass of molecular ion: 140)
Source Temperature: 260 °C Sample Temperature: 170 °C Reservoir, 75 eV
18.0 4.1 26.0 5.2 27.0 9.7 28.0 8.3 31.0 1.0 32.0 1.5 39.0 1.3 40.0 1.3 41.0 4.3 42.0 4.0 45.0 15.3 46.0 6.9 47.0 9.7 51.0 2.1 52.0 5.8 53.0 2.6 54.0 100.0 55.0 5.8 57.0 2.2 58.0 3.0 59.0 6.5 60.0 4.2 72.0 1.9 73.0 5.3 86.0 1.1 100.0 54.5 101.0 3.2 102.0 2.6 113.0 5.0 140.0 22.2 141.0 1.9 142.0 1.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H8 N2 S 0.04 ml : 0.5 ml CDCl3 3,3'-thiodipropionitrile 
Assign. Shift(ppm)
A 2.89 B 2.72
Hz ppm Int.269.06 3.005 149 266.06 2.971 209 263.94 2.948 179 260.19 2.906 394 259.63 2.899 1000 257.25 2.873 43 256.69 2.867 37 255.13 2.849 596 254.00 2.837 704 251.19 2.805 33 248.06 2.770 691 246.94 2.758 601 245.06 2.737 43 244.06 2.726 32 242.38 2.707 922 241.81 2.700 374 238.06 2.659 179 235.94 2.635 210 232.94 2.601 152
in CDCl3
KBr disc
liquid film
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