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网站主页CAS数据库列表 111-97-7更多图谱硫代丙二腈(111-97-7)红外图谱(IR3)

硫代丙二腈

产品名称 硫代丙二腈

CAS号111-97-7

分子式C6H8N2S

分子量140.21

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  • Mass

    MS-NW-1454          
    3,3'-thiodipropionitrile
    C6H8N2S             (Mass of molecular ion:    140)
    

       Source Temperature: 260 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          18.0       4.1
          26.0       5.2
          27.0       9.7
          28.0       8.3
          31.0       1.0
          32.0       1.5
          39.0       1.3
          40.0       1.3
          41.0       4.3
          42.0       4.0
          45.0      15.3
          46.0       6.9
          47.0       9.7
          51.0       2.1
          52.0       5.8
          53.0       2.6
          54.0     100.0
          55.0       5.8
          57.0       2.2
          58.0       3.0
          59.0       6.5
          60.0       4.2
          72.0       1.9
          73.0       5.3
          86.0       1.1
         100.0      54.5
         101.0       3.2
         102.0       2.6
         113.0       5.0
         140.0      22.2
         141.0       1.9
         142.0       1.2
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H8 N2 S 0.04 ml : 0.5 ml CDCl3
    3,3'-thiodipropionitrile
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.89 B 2.72

         Hz     ppm     Int.
    

        269.06   3.005    149
        266.06   2.971    209
        263.94   2.948    179
        260.19   2.906    394
        259.63   2.899   1000
        257.25   2.873     43
        256.69   2.867     37
        255.13   2.849    596
        254.00   2.837    704
        251.19   2.805     33
        248.06   2.770    691
        246.94   2.758    601
        245.06   2.737     43
        244.06   2.726     32
        242.38   2.707    922
        241.81   2.700    374
        238.06   2.659    179
        235.94   2.635    210
        232.94   2.601    152
    

in CDCl3



KBr disc



liquid film



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