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网站主页CAS数据库列表 111-27-3更多图谱正己醇(111-27-3)核磁图(13CNMR)

正己醇

产品名称 正己醇

CAS号111-27-3

分子式C6H14O

分子量102.17

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  • Mass

    MS-NW-0547          
    hexyl alcohol
    C6H14O              (Mass of molecular ion:    102)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       1.1
          18.0       2.6
          26.0       1.0
          27.0      14.9
          28.0       3.1
          29.0      19.8
          31.0      23.7
          39.0       8.5
          40.0       1.9
          41.0      36.0
          42.0      43.4
          43.0      59.0
          44.0       2.1
          45.0       2.9
          53.0       1.5
          54.0       2.7
          55.0      48.9
          56.0     100.0
          57.0       7.1
          69.0      25.1
          70.0       3.4
          71.0       1.7
          73.0       1.3
          83.0       1.5
          84.0       8.6
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H14 O 0.04 ml : 0.5 ml CDCl3
    hexyl alcohol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.624 B 1.79 C 1.56 D 1.32 E 0.90

         Hz     ppm     Int.
    

        331.25   3.699    136
        328.31   3.666     37
        324.75   3.627    440
        318.38   3.555    210
        160.38   1.791   1000
        148.31   1.656     31
        146.63   1.638     52
        145.38   1.624     44
        144.94   1.619     44
        144.19   1.610     41
        143.38   1.601     42
        140.44   1.569     84
        139.25   1.555     78
        138.81   1.550     78
        137.13   1.532     62
        134.31   1.500     85
        133.69   1.493     81
        133.13   1.487     84
        131.94   1.474     71
        129.44   1.446     90
        127.50   1.424    115
        125.31   1.400    133
        125.00   1.396    134
        121.19   1.354    250
        120.88   1.350    250
        119.56   1.335    317
        118.69   1.326    311
        118.06   1.319    324
        116.88   1.306    320
        115.69   1.292    328
        108.69   1.214     62
         87.31   0.975     71
         85.50   0.955    116
         83.13   0.929     96
         80.06   0.894    436
         75.69   0.846     62
         74.06   0.827     82
         73.13   0.817     70
         72.56   0.811     73
         70.06   0.783     31
    

in CDCl3



CCl4 solution



liquid film



4880 A,100M,liquid