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网站主页CAS数据库列表 111-01-3更多图谱角鲨烷(111-01-3)核磁图(13CNMR)

角鲨烷

产品名称 角鲨烷

CAS号111-01-3

分子式C30H62

分子量422.81

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  • Mass

    MS-NW-2144          
    2,6,10,15,19,23-hexamethyltetracosane
    C30H62              (Mass of molecular ion:    422)
    

       Source Temperature: 210 °C
       Sample Temperature: 160 °C
       Direct, 75 eV
    

          18.0       1.8
          27.0       1.4
          28.0       1.1
          29.0       5.6
          39.0       1.1
          41.0      14.0
          42.0       3.3
          43.0      42.4
          44.0       1.5
          55.0      17.8
          56.0      17.4
          57.0     100.0
          58.0       4.4
          67.0       1.5
          68.0       1.7
          69.0      14.6
          70.0      11.2
          71.0      78.3
          72.0       4.2
          81.0       1.6
          82.0       1.9
          83.0       8.9
          84.0       6.9
          85.0      44.0
          86.0       3.0
          95.0       1.7
          96.0       3.3
          97.0       9.8
          98.0       3.7
          99.0      25.6
         100.0       1.9
         109.0       1.0
         110.0       2.8
         111.0       9.8
         112.0      20.7
         113.0      34.7
         114.0       2.9
         125.0       4.2
         126.0      10.0
         127.0      21.0
         128.0       2.1
         139.0       1.5
         140.0       2.8
         141.0      14.0
         142.0       1.5
         153.0       1.2
         154.0       3.5
         155.0      12.7
         156.0       1.5
         169.0       9.3
         170.0       1.2
         181.0       2.1
         182.0      13.1
         183.0      24.9
         184.0       3.2
         196.0       3.2
         197.0       7.1
         211.0       5.4
         225.0       3.8
         238.0       8.5
         239.0      16.9
         240.0       3.1
         253.0       2.2
         266.0       6.5
         267.0       8.3
         268.0       1.5
         281.0       1.3
         308.0       1.7
         309.0       1.7
         336.0       2.9
         337.0       4.4
         338.0       1.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C30 H62 0.05 ml 0.5 ml CDCl3
    2,6,10,15,19,23-hexamethyltetracosane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.519 B 1.37 C 1.26 D 1.15 E 1.08 F 0.868 G 0.845

         Hz     ppm     Int.
    

        622.80   1.559     44
        616.21   1.542     86
        609.62   1.526    110
        603.03   1.509     94
        596.31   1.493     60
        546.63   1.368     91
        501.46   1.255    363
        458.25   1.147    132
        431.27   1.080    165
        350.22   0.877    994
        343.51   0.860   1000
        340.82   0.853    802
        334.23   0.837    730
    

in CDCl3



CCl4 solution



liquid film