-
MassMS-NW-5520 cyclohexanol C6H12O (Mass of molecular ion: 100)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.4 18.0 1.7 26.0 1.3 27.0 11.4 28.0 3.5 29.0 10.1 31.0 5.9 38.0 1.0 39.0 11.4 40.0 2.2 41.0 22.7 42.0 7.4 43.0 6.9 44.0 24.0 45.0 4.0 50.0 1.1 51.0 1.6 53.0 4.1 54.0 14.8 55.0 8.1 56.0 13.2 57.0 100.0 58.0 8.7 67.0 26.5 68.0 1.8 69.0 1.8 70.0 1.2 71.0 13.2 72.0 7.0 79.0 1.7 81.0 5.4 82.0 46.1 83.0 4.1 85.0 1.0 99.0 1.4 100.0 3.3
90 MHz in CDCl3
400 MHz in CDCl3
-
1H NMR 89.56 MHz C6 H12 O 10.3 mol% in CDCl3 cyclohexanol 
Assign. Shift(ppm)
A 3.58 B 2.63 C 1.04 to 2.04 400MHZ : HSP-40-238
Hz ppm Int.331.00 3.696 30 326.38 3.645 45 325.44 3.634 49 324.50 3.624 48 321.63 3.592 68 319.44 3.567 48 318.63 3.558 52 317.31 3.543 66 315.94 3.528 50 313.75 3.504 40 313.00 3.495 37 312.00 3.484 46 235.56 2.631 1000 179.50 2.005 37 178.25 1.991 48 174.50 1.949 84 172.63 1.928 105 170.50 1.904 142 169.56 1.894 151 168.69 1.884 145 167.38 1.869 152 166.50 1.860 147 165.81 1.852 148 163.25 1.823 138 161.00 1.798 163 160.06 1.788 158 158.63 1.772 183 156.69 1.750 156 155.06 1.732 181 154.06 1.721 181 148.44 1.658 87 147.38 1.646 83 145.94 1.630 83 145.81 1.629 83 144.81 1.617 83 143.31 1.601 94 142.63 1.593 99 141.63 1.582 100 140.63 1.571 97 140.06 1.564 98 138.75 1.550 101 137.63 1.537 99 134.13 1.498 81 131.19 1.465 92 130.88 1.462 93 130.38 1.456 95 129.69 1.449 91 129.56 1.447 91 128.88 1.440 91 128.75 1.438 91 126.69 1.415 90 126.25 1.410 90 121.75 1.360 154 118.81 1.327 178 114.38 1.278 293 113.31 1.266 334 110.75 1.237 298 109.13 1.219 263 107.38 1.199 202 105.75 1.181 223 105.00 1.173 222 99.81 1.115 67 99.44 1.111 66
-
1H NMR 399.65 MHz C6 H12 O 0.05 ml : 0.5 ml CDCl3 cyclohexanol Assign. Shift(ppm)
A 3.578 B 2.84 C 1.882 D 1.728 E 1.542 F 1.30 to 1.22 G 1.16
Hz ppm Int.1443.48 3.612 49 1439.21 3.602 79 1434.08 3.589 131 1429.93 3.578 156 1425.54 3.567 129 1422.49 3.560 76 1420.53 3.555 85 1416.50 3.545 39 1134.40 2.839 1000 761.60 1.906 131 756.71 1.894 266 753.66 1.886 272 752.56 1.884 276 749.88 1.877 228 748.66 1.874 226 743.53 1.861 158 700.93 1.754 120 697.39 1.746 176 692.87 1.734 223 691.89 1.732 233 688.84 1.724 327 685.18 1.715 235 683.96 1.712 217 679.69 1.701 92 673.95 1.687 45 672.36 1.683 36 625.37 1.565 95 623.54 1.561 107 622.44 1.558 126 621.34 1.555 112 619.38 1.550 100 617.19 1.545 82 615.84 1.541 97 614.38 1.538 101 613.04 1.534 102 610.35 1.528 132 608.15 1.522 102 606.93 1.519 109 603.39 1.510 42 602.42 1.508 40 529.05 1.324 61 525.76 1.316 62 521.48 1.305 78 517.46 1.295 162 512.94 1.284 254 511.84 1.281 267 508.06 1.272 319 504.64 1.263 539 502.69 1.258 527 496.95 1.244 289 493.04 1.234 408 483.76 1.211 111 482.18 1.207 110 479.25 1.200 100 475.83 1.191 86 474.00 1.187 77 470.21 1.177 84 466.80 1.169 105 464.23 1.162 103 458.62 1.148 79 455.20 1.139 81 451.66 1.131 64 447.27 1.120 32 443.73 1.111 30
in CDCl3
CCl4 solution
liquid film
4880 A,200 M,liquid
更多供应商
