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MassMS-IW-8616 3-(trichlorosilyl)propionitrile C3H4Cl3NSi (Mass of molecular ion: 187)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 1.8 27.0 3.4 28.0 9.8 36.0 3.2 38.0 1.1 49.0 1.9 51.0 1.4 52.0 2.3 53.0 1.4 54.0 9.7 58.0 3.6 63.0 20.2 64.0 1.5 65.0 7.5 86.0 1.4 98.0 14.6 99.0 3.3 100.0 10.0 101.0 2.1 102.0 2.0 112.0 1.0 124.0 6.2 125.0 1.7 126.0 4.3 133.0 97.4 134.0 5.1 135.0 98.1 136.0 4.9 137.0 34.0 138.0 1.6 139.0 4.4 147.0 2.2 149.0 2.3 151.0 1.9 152.0 2.8 153.0 1.2 154.0 1.9 160.0 6.0 162.0 5.8 164.0 2.0 186.0 99.4 187.0 9.5 188.0 100.0 189.0 9.1 190.0 34.5 191.0 3.1 192.0 4.5 266.0 1.3 268.0 1.8 270.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C3 H4 Cl3 N Si 0.048 g : 0.5 ml CDCl3 3-(trichlorosilyl)propionitrile 
Assign. Shift(ppm)
A 2.626 B 1.823
Hz ppm Int.1061.89 2.658 51 1058.11 2.648 856 1053.10 2.636 242 1051.15 2.631 520 1050.05 2.628 913 1048.34 2.624 425 1046.51 2.619 238 1041.87 2.607 1000 741.21 1.855 43 736.57 1.844 950 731.81 1.832 239 729.86 1.827 447 728.39 1.823 867 727.05 1.820 449 725.22 1.815 213 723.63 1.811 57 720.34 1.803 856 715.58 1.791 29
in CDCl3
KBr disc
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