90 MHz in D2O
-
1H NMR 89.56 MHz C3 H10 N2 0.051 g : 0.5 ml D2O trimethylenediamine dihydrochloride 
Assign. Shift(ppm)
A 3.148 B 2.114 SOLVENT PEAK REMOVED
Hz ppm Int.294.94 3.294 35 294.56 3.289 36 289.56 3.234 625 286.94 3.204 115 281.88 3.148 1000 279.00 3.116 412 274.06 3.061 982 269.44 3.009 51 268.06 2.994 37 267.69 2.989 34 267.44 2.987 34 266.94 2.981 32 203.63 2.274 131 197.69 2.208 178 195.56 2.184 215 194.31 2.170 252 190.50 2.128 175 187.69 2.096 348 181.94 2.032 148 179.63 2.006 165 178.31 1.991 171 172.69 1.929 69
in D2O
KBr disc
nujol mull
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