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MassMS-NW-9259 S-(-)-1-(1-naphthyl)ethylamine C12H13N (Mass of molecular ion: 171)
Source Temperature: 250 °C Sample Temperature: 160 °C Reservoir, 75 eV
28.0 2.6 42.0 5.1 43.0 4.1 44.0 10.0 51.0 2.2 63.0 2.7 64.0 1.7 65.0 2.5 71.5 1.7 74.0 1.0 75.0 1.9 76.0 2.7 76.5 2.3 77.0 6.9 77.5 5.3 78.0 11.3 78.5 1.2 83.5 1.8 84.5 3.2 101.0 1.7 102.0 1.5 115.0 2.2 126.0 3.4 127.0 12.5 128.0 19.0 129.0 39.0 130.0 4.8 139.0 1.1 141.0 1.3 151.0 1.9 152.0 5.6 153.0 7.9 154.0 8.8 155.0 4.4 156.0 100.0 157.0 12.1 167.0 1.1 168.0 1.8 170.0 5.6 171.0 17.1 172.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H13 N 0.05 ml : 0.5 ml CDCl3 S-(-)-1-(1-naphthyl)ethylamine 
Assign. Shift(ppm)
A 8.093 B 7.833 C 7.707 D 7.611 E *1 7.487 F *1 7.45 G 7.44 J 4.895 K 1.57 L 1.502 ASSIGNED BY H-H COSY.
Hz ppm Int.3239.01 8.105 132 3230.59 8.084 142 3135.13 7.845 119 3134.40 7.843 114 3133.67 7.842 111 3127.32 7.826 146 3125.61 7.821 142 3084.47 7.718 142 3076.29 7.698 167 3045.78 7.622 144 3038.57 7.604 174 3001.59 7.511 68 3000.12 7.507 82 2994.87 7.494 140 2993.29 7.490 167 2991.70 7.486 79 2986.57 7.473 154 2984.86 7.469 142 2982.67 7.464 152 2980.96 7.459 265 2975.83 7.447 93 2974.49 7.443 181 2973.27 7.440 305 2967.90 7.427 80 2966.55 7.423 81 2965.21 7.420 136 1966.43 4.921 49 1959.84 4.904 144 1953.25 4.888 146 1946.66 4.871 52 625.85 1.566 100 625.24 1.565 100 624.39 1.563 98 617.55 1.546 55 612.18 1.532 35 610.96 1.529 39 603.88 1.512 980 597.29 1.495 1000
KBr disc
liquid film
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