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MS-NW-5868 4-methoxy-2-methylaniline C8H11NO (Mass of molecular ion: 137)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.3 27.0 2.0 28.0 4.1 38.0 1.6 39.0 6.2 40.0 1.3 41.0 3.8 42.0 2.3 50.0 1.8 51.0 4.3 52.0 5.2 53.0 4.0 54.0 3.9 63.0 1.8 65.0 3.8 66.0 5.0 67.0 4.8 68.0 1.4 77.0 12.7 78.0 2.8 79.0 2.5 92.0 1.5 93.0 10.5 94.0 24.6 95.0 1.9 106.0 1.8 121.0 1.1 122.0 100.0 123.0 8.5 136.0 3.1 137.0 74.6 138.0 6.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H11 N O 0.05 ml : 0.5 ml CDCl3 4-methoxy-2-methylaniline Assign. Shift(ppm)
A 6.638 B 6.588 C 6.555 D 3.688 E 3.33 F 2.103
Hz ppm Int.
2654.17 6.642 147 2651.98 6.636 157 2651.37 6.635 180 2640.38 6.607 70 2637.57 6.600 41 2631.84 6.586 163 2629.03 6.579 137 2625.24 6.569 40 2621.95 6.561 281 2613.53 6.540 107 1474.12 3.689 1000 1329.10 3.326 45 840.58 2.104 709
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