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MassMS-IW-0849 methyl 3,4,5-trimethoxyanthranilate C11H15NO5 (Mass of molecular ion: 241)
Source Temperature: 150 °C Sample Temperature: 100 °C Direct, 75 eV
15.0 2.8 28.0 1.1 52.0 3.9 53.0 4.0 65.0 1.4 66.0 1.2 68.0 1.1 80.0 1.6 81.0 2.0 93.0 1.7 94.0 1.0 95.0 2.3 96.0 1.3 108.0 1.5 110.0 1.8 112.0 3.0 120.5 1.9 121.0 1.0 122.0 1.1 123.0 2.4 124.0 1.5 136.0 1.4 138.0 2.3 140.0 1.7 148.0 2.0 150.0 1.9 151.0 7.1 152.0 2.5 164.0 1.5 165.0 1.4 166.0 15.8 167.0 7.1 168.0 1.3 176.0 1.0 178.0 1.3 179.0 2.9 180.0 1.4 181.0 4.1 183.0 1.2 194.0 48.9 195.0 5.4 208.0 4.5 209.0 2.2 210.0 6.5 211.0 2.4 226.0 65.2 227.0 7.6 228.0 1.1 241.0 100.0 242.0 12.7 243.0 1.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H15 N O5 0.038 g : 0.5 ml CDCl3 methyl 3,4,5-trimethoxyanthranilate 
Assign. Shift(ppm)
A 7.149 B 5.72 C 3.953 D *1 3.864 E *1 3.863 F *1 3.811
Hz ppm Int.2857.06 7.149 260 2285.64 5.720 38 1579.83 3.954 914 1544.56 3.865 991 1543.95 3.864 1000 1523.32 3.812 743
in CDCl3
KBr disc
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