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MassMS-NW-0560 N-ethyl-m-toluidine C9H13N (Mass of molecular ion: 135)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.6 28.0 1.8 29.0 1.6 39.0 5.0 41.0 2.7 42.0 1.6 43.0 1.6 50.0 1.5 51.0 3.2 52.0 1.8 53.0 1.3 58.5 1.0 59.5 1.8 60.0 1.5 63.0 2.6 64.0 1.0 65.0 7.7 77.0 6.6 78.0 2.4 79.0 2.9 80.0 1.0 89.0 2.0 90.0 1.5 91.0 17.8 92.0 5.0 93.0 3.3 104.0 1.4 105.0 1.1 106.0 2.2 117.0 1.0 118.0 3.7 119.0 3.2 120.0 100.0 121.0 9.3 134.0 6.6 135.0 37.2 136.0 3.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H13 N 0.05 ml : 0.5 ml CDCl3 N-ethyl-m-toluidine 
Assign. Shift(ppm)
A 7.038 B 6.502 C 6.387 D 6.38 E 3.33 F 3.084 G 2.254 J 1.186
Hz ppm Int.2821.29 7.060 104 2818.97 7.054 48 2813.84 7.041 144 2812.50 7.038 124 2811.16 7.035 57 2807.62 7.026 33 2805.05 7.019 132 2602.66 6.513 138 2602.17 6.512 135 2594.97 6.494 127 2594.24 6.492 114 2552.86 6.388 330 2546.26 6.372 125 2543.95 6.366 67 1332.40 3.334 36 1243.41 3.112 173 1236.33 3.094 484 1229.13 3.076 482 1221.92 3.058 176 901.12 2.255 1000 481.08 1.204 571 474.00 1.187 960 466.80 1.169 511
in CDCl3
CCl4 solution
liquid film
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