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网站主页CAS数据库列表 102-27-2更多图谱N-乙基间甲苯胺(102-27-2)核磁图(13CNMR)

N-乙基间甲苯胺

产品名称 N-乙基间甲苯胺

CAS号102-27-2

分子式C9H13N

分子量135.21

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  • Mass

    MS-NW-0560          
    N-ethyl-m-toluidine
    C9H13N              (Mass of molecular ion:    135)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       2.6
          28.0       1.8
          29.0       1.6
          39.0       5.0
          41.0       2.7
          42.0       1.6
          43.0       1.6
          50.0       1.5
          51.0       3.2
          52.0       1.8
          53.0       1.3
          58.5       1.0
          59.5       1.8
          60.0       1.5
          63.0       2.6
          64.0       1.0
          65.0       7.7
          77.0       6.6
          78.0       2.4
          79.0       2.9
          80.0       1.0
          89.0       2.0
          90.0       1.5
          91.0      17.8
          92.0       5.0
          93.0       3.3
         104.0       1.4
         105.0       1.1
         106.0       2.2
         117.0       1.0
         118.0       3.7
         119.0       3.2
         120.0     100.0
         121.0       9.3
         134.0       6.6
         135.0      37.2
         136.0       3.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H13 N 0.05 ml : 0.5 ml CDCl3
    N-ethyl-m-toluidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.038 B 6.502 C 6.387 D 6.38 E 3.33 F 3.084 G 2.254 J 1.186

         Hz     ppm     Int.
    

       2821.29   7.060    104
       2818.97   7.054     48
       2813.84   7.041    144
       2812.50   7.038    124
       2811.16   7.035     57
       2807.62   7.026     33
       2805.05   7.019    132
       2602.66   6.513    138
       2602.17   6.512    135
       2594.97   6.494    127
       2594.24   6.492    114
       2552.86   6.388    330
       2546.26   6.372    125
       2543.95   6.366     67
       1332.40   3.334     36
       1243.41   3.112    173
       1236.33   3.094    484
       1229.13   3.076    482
       1221.92   3.058    176
        901.12   2.255   1000
        481.08   1.204    571
        474.00   1.187    960
        466.80   1.169    511
    

in CDCl3



CCl4 solution



liquid film