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网站主页CAS数据库列表 101-86-0更多图谱α-己基肉桂醛(101-86-0)核磁图(13CNMR)

α-己基肉桂醛

产品名称 α-己基肉桂醛

CAS号101-86-0

分子式C15H20O

分子量216.32

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  • Mass

    MS-IW-6337          
    alpha-hexylcinnamaldehyde
    C15H20O             (Mass of molecular ion:    216)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       5.7
          29.0       7.6
          39.0       7.8
          41.0      12.0
          42.0       1.2
          43.0      11.1
          50.0       1.2
          51.0       4.9
          52.0       1.3
          53.0       3.2
          54.0       1.2
          55.0       8.4
          57.0       2.9
          63.0       3.2
          65.0       5.7
          67.0       5.1
          68.0       1.5
          69.0       3.0
          71.0       1.4
          75.0       1.2
          76.0       1.7
          77.0       9.0
          78.0       6.8
          79.0       3.3
          81.0       3.4
          82.0      11.3
          83.0      10.4
          84.0       1.3
          89.0       3.8
          91.0      53.7
          92.0       8.1
          93.0       1.2
          95.0       6.3
          96.0       2.3
          97.0       1.6
          99.0       1.6
         102.0       3.4
         103.0       4.9
         104.0       9.5
         105.0       8.1
         107.0       2.7
         109.0       1.7
         115.0      41.1
         116.0      22.7
         117.0      63.5
         118.0      12.8
         119.0       1.7
         120.0       1.9
         125.0       5.0
         126.0       1.0
         127.0       7.2
         128.0      15.0
         129.0     100.0
         130.0      22.2
         131.0      33.4
         132.0       8.1
         133.0       3.4
         139.0       1.3
         141.0      13.3
         142.0       5.0
         143.0       6.4
         144.0       3.2
         145.0      43.8
         146.0      10.5
         147.0       2.3
         153.0       1.6
         154.0       1.0
         155.0       7.0
         156.0       1.8
         157.0       1.4
         158.0       4.6
         159.0      14.7
         160.0       3.3
         165.0       2.0
         167.0       1.5
         169.0       5.6
         170.0       1.0
         173.0      15.2
         174.0      11.2
         175.0       1.4
         185.0       3.1
         187.0       2.0
         198.0       2.6
         200.0       4.9
         201.0       1.1
         215.0      22.9
         216.0      44.9
         217.0       7.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C15 H20 O 0.05 ml : 0.5 ml CDCl3
    alpha-hexylcinnamaldehyde
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.34 B 7.476 C 7.439 D 7.388 E 7.191 F 2.521 G 1.487 J 1.37 K 1.29 L 0.879

         Hz     ppm     Int.
    

       3810.96   9.536    867
       2999.53   7.506    237
       2997.89   7.502    326
       2995.87   7.497    147
       2990.74   7.484    589
       2990.01   7.482    551
       2987.81   7.477    138
       2981.40   7.461    261
       2979.94   7.457    352
       2977.92   7.452    146
       2974.99   7.444    186
       2972.98   7.439    662
       2971.14   7.435    271
       2966.93   7.424    205
       2965.47   7.421    326
       2963.27   7.415     91
       2959.97   7.407    197
       2958.51   7.403    324
       2956.86   7.399    185
       2954.11   7.392    126
       2951.36   7.385    302
       2948.25   7.378    105
       2945.50   7.371     96
       2944.40   7.368    128
       2942.94   7.364    110
       2941.65   7.361     52
       2874.25   7.192    644
       1016.21   2.543    310
       1008.51   2.524    318
       1006.32   2.519    200
       1000.27   2.503    348
        610.86   1.529     65
        609.94   1.527     63
        603.53   1.511    167
        601.15   1.505    128
        599.14   1.500    134
        595.11   1.490    253
        590.71   1.479    174
        587.78   1.471    227
        585.03   1.464    153
        580.09   1.452    114
        562.69   1.408     70
        556.28   1.392    172
        554.81   1.389    164
        549.87   1.376    196
        548.58   1.373    200
        547.30   1.370    198
        541.26   1.355    170
        534.66   1.338    120
        532.46   1.333    111
        528.07   1.322    167
        521.11   1.304    590
        517.08   1.294    522
        514.15   1.287    664
        511.03   1.279    374
        507.00   1.269    237
        501.51   1.255     60
        357.72   0.896    374
        356.63   0.893    345
        355.34   0.890    261
        350.76   0.878   1000
        345.82   0.866    233
        343.62   0.860    335
        335.74   0.841     41
    

in CDCl3



liquid film